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Id7 diamond attenuated total reflectance

Manufactured by Thermo Fisher Scientific

The ID7 diamond attenuated total reflectance is a spectroscopic accessory designed for infrared (IR) analysis. It utilizes a diamond crystal to facilitate the attenuated total reflectance (ATR) technique, which allows for the examination of solid, liquid, and semi-solid samples without the need for complex sample preparation.

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2 protocols using id7 diamond attenuated total reflectance

1

Structural Analysis of Modified Silk

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The structural conformations of modified silks (either as lyophilized powders or films) were analyzed with a Nicolet iS5 FT-IR equipped with an iD7 diamond attenuated total reflectance (ATR) accessory (Thermo Scientific, Waltham, MA). The absorbance of samples was measured between 4000 – 400 cm−1, with 64 scans, and a resolution of 4 cm−1. Background spectra were collected under the same conditions and subtracted from the sample. All samples were analyzed after 24 hours with or without methanol (100% v/v) treatment.
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2

Structural Analysis of Modified Substructures

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The structural conformations of modified substructure solutions, were analyzed with a Nicolet iS5 FT-IR equipped with an iD7 diamond attenuated total reflectance (ATR) accessory (Thermo Scientific, Waltham, MA). The absorbance of M300 and M150 samples, respectively, with or without methanol treatment, was measured between 4000 – 400 cm−1, with 64 scans, and a resolution of 4 cm−1. Background spectra were collected under the same conditions and subtracted from the sample. All samples were analyzed after 24 hours with or without methanol (100% v/v; 1:1 v/v ratio to substructure solution) treatment.
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