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Benzyl bromide

Manufactured by Fujifilm
Sourced in Japan

Benzyl bromide is a colorless, volatile liquid used as a chemical intermediate in various industrial processes. It is a versatile compound that serves as a building block for the synthesis of other organic compounds. Benzyl bromide exhibits high reactivity and is commonly employed in organic synthesis reactions.

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3 protocols using benzyl bromide

1

Lipid Synthesis and Purification

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DPPC and DOPC were purchased
from Avanti Polar Lipid (Alabaster, AL). CTAB, sodium hydroxide,
and benzyl bromide were purchased from Wako Pure Chemicals (Osaka,
Japan). DDAB, TBAH, and DMGBE were purchased from Tokyo Chemical
Industries (Tokyo, Japan). All of these chemicals were used without
further purification.
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2

Synthesis of Tri-6-O-mesitylenesulfonyl-α-CD

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The α-CD was supplied by Ensuiko Sugar Refining Co., Ltd., and dried overnight in vacuo at 110 °C before use. TrCl (Tokyo Chemical Industry Co., Ltd.), benzyl bromide and mesitylenesulfonyl chloride (Wako Pure Chemical Industries Ltd.) were used without further purification. Commercially available NaH in oil (50–77%) and Pd/C (Pd 10%) were used for the conversion of tri-6-O-trityl-α-CD to tri-6-O-mesitylenesulfonyl-α-CD. Reagent-grade pyridine was dried over CaH2 and distilled in the presence of CaH2 before use. N,N-Dimethylformamide (DMF) was also dried over CaH2 and distilled before use. Acetonitrile for high performance liquid chromatography was purchased from Wako Pure Chemical Industries Ltd. DMSO-d6 containing 0.05% v/v tetramethylsilane (Cambridge Isotope Laboratiories, Inc., 99.9 atom % D) was used for 1H NMR measurements.
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3

Perfluoroalkyl Substances Quantification

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Perfluorooctanoic acid (PFOA, C8), perfluorononanoic acid (PFNA, C9), perfluorodecanoic acid (PFDA, C10), perfluoroundecanoic acid (PFUnDA, C11), and perfluorododecanoic acid (PFDoDA, C12), perfluorotetradecanoic acid (PFTeDA, C14), cyclosporin A, sodium azide (NaN3), 2,4-dinitrophenol (DNP), Dulbecco's modified Eagle's medium (DMEM), tetrabutylammonium hydrogen sulfate and benzyl bromide were purchased from Wako Pure Chemical Industries, Ltd. (Osaka, Japan). Perfluoropropionic acid (PFPrA, C3), perfluorobutanoic acid (PFBA, C4), perfluoropentanoic acid (PFPeA, C5), Perfluorohexanoic acid (PFHxA, C6), perfluoroheptanoic acid (PFHpA, C7), HPLC grade methanol and methyl tert-butyl ether (MTBE) were obtained from Kanto Chemicals Co., Ltd. (Tokyo, Japan). Perfluorotridecanoic acid (PFTrDA, C13), sulfobromophthalein (BSP) and glibenclamide were purchased from Sigma-Aldrich (St. Louis, MO). Fetal bovine serum (FBS) and nonessential amino acid (NEAA) were obtained from Life Technologies Co. (Carlsbad, CA). A mixture of 13C2-labeled PFHxA, 13C4-labeled PFOA, 13C5-labeled PFNA, 13C2-labeled PFDA, 13C2-labeled PFUnDA and 13C2-labeled PFDoDA were purchased from Wellington Laboratories Inc. (MPFAX-MXA; Guelph, Canada). All other chemicals used were of the highest purity commercially available.
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