Nickel chloride hexahydrate

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Nickel chloride hexahydrate is an inorganic compound with the chemical formula NiCl2·6H2O. It is a green crystalline solid that is commonly used as a source of nickel ions in various applications.

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Nickel (II) Chloride-hexahydrate (11 citations)

5 protocols using nickel chloride hexahydrate

Synthesis of Carbon-Supported Nickel Catalyst

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Commercial TiC (d_ave of 90 µm, 99.8%, Goodfellow) was employed as carbon precursor. Chlorine (purity 2.8, Linde AG) and hydrogen (purity 5.0, Linde AG) diluted by helium (purity 4.6, Linde AG) were used to perform reactive extraction of carbide (chlorination) and subsequent carbon surface annealing. Nickel chloride hexahydrate (99.95% purity, Alfa Aesar) was used as precursor of the Ni catalyst.

Ariyanto T., Glaesel J., Kern A., Zhang G.R, & Etzold B.J. (2019). Improving control of carbide-derived carbon microstructure by immobilization of a transition-metal catalyst within the shell of carbide/carbon core–shell structures. Beilstein Journal of Nanotechnology, 10, 419-427.

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Fabrication of Yttrium-Doped Barium Cerate Anode

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Yttrium-doped barium cerate powder BaCe₀.₈₅Y₀.₁₅O₂.₉₂₅ (BCY15), supplied by Marion Technologies, was fabricated by auto-combustion method and applied as the anode ceramic matrix. Before synthesis, the BCY15 powder was thermally pretreated at 1100 °C for 2 h. Nickel chloride hexahydrate (NiCl₂·6H₂O), hydrazine monohydrate (99+% N₂H₄·H₂O), sodium hydroxide (NaOH), and anhydrous sodium carbonate (Na₂CO₃) were procured by Alfa Aesar (Ward Hill, MA, USA). Anhydrous (99.8%) ethylene glycol (EG) was acquired by SIGMA-ALDRICH. All reagents were of “pro analyze” purity grade and were used as received without further purification.

Gabrovska M., Nikolova D., Kolev H., Karashanova D., Tzvetkov P., Burdin B., Mladenova E., Vladikova D, & Tabakova T. (2023). Environmentally Benign pSOFC for Emissions-Free Energy: Assessment of Nickel Network Resistance in Anodic Ni/BCY15 Nanocatalyst. Nanomaterials, 13(11), 1781.

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Electrochemical Characterization of Metal Foils

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Aluminum foils (Al, 99.997%) and Nickel chloride hexahydrate (NiCl₂·6H₂O, 99.3%) were purchased from Alfa Aesar. Perchloric acid (HClO₄, 70%), and Potassium dichromate (K₂Cr₂O₇, 99.5%) were purchased from Sigma-Aldrich. Oxalic acid dihydrate (C₂H₂O₄·2H₂O, 99.5%), Sodium hydroxide (NaOH, 97%) and copper sulfate (CuSO₄, 99.5%) were purchased from Showa Kako. Hydrochloric acid (HCl, 37%) was purchased from Scharlau. Phosphoric acid (H₃PO₄, 72%) was purchased from J.T. Baker® chemicals. Acetone (C₃H₆O, 99%), isopropyl alcohol (C₃H₇OH, 99%), and anhydrous ethanol (C₂H₅OH, 99.5%) were purchased from Echo Chemical. Epoxy quickstick was purchased from EMS. The deionized water was obtained from the EASYpure® II system. All the materials were used as received without further purification.

Huang C.L., Weng W.L., Liao C.N, & Tu K.N. (2018). Suppression of interdiffusion-induced voiding in oxidation of copper nanowires with twin-modified surface. Nature Communications, 9, 340.

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Comprehensive Chemical Reagent Acquisition

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Aluminium chloride (99%), ammonium bicarbonate (≥99.5%), L-aspartic acid disodium salt (≥98%), L-alanine (≥99.5), β-alanine (≥99%), calcium chloride dihydrate (≥99%), chloroform (100–200 ppm amylene stabiliser, ≥99.5), cobalt chloride hexahydrate (cell culture grade), glycine (≥99%), glutamate (≥99%), guanidine chloride solution (8 M), hydrochloric acid (≥37%), isobutyl chloroformate (98%), manganese sulfate (cell culture grade), oxaloacetic acid (≥97%), potassium chloride (99%), potassium phosphate monobasic (99.5–101.0%), pyridine (98%), pyridoxamine dihydrochloride (cell culture grade), pyridoxal hydrochloride (≥99%), L-serine (≥99%), sodium acetate (99–101%), sodium orthovanadate (99.98%), and zinc chloride x (≥98%) were purchased from Sigma. Boric acid (analytical grade), water (HPLC grade) and acetonitrile (HPLC grade) were purchased from Fischer. Copper sulfate hexahydrate (98.0–102.0%), isobutanol (99%), magnesium chloride hexahydrate (≥98%), and nickel chloride hexahydrate (98%) were from Alfa Aesar. Sodium hydroxide was purchased from VWR, and sodium chloride (research-grade) was purchased from Millipore. Ammonium chloride (analysis-grade) was from Acros and 9-fluroenylmethoxycarbonyl chloride (97%) was from Novabiochem. Helium (99.995%) and Nitrogen (99.998%) were purchased from BOC.

Harrison S.A., Webb W.L., Rammu H, & Lane N. (2023). Prebiotic Synthesis of Aspartate Using Life’s Metabolism as a Guide. Life, 13(5), 1177.

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Synthesis of Nanostructured Metal-Polymer Composites

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Poly(ethersulfone) (PES) Ultrason E 6020P (glass transition temperature T_g = 225 °C and a molecular weight (Mw) of 58,000 g/mol, polymer density = 1.37 g/cm³) was obtained from BASF chemical company (Ludwigshafen, Germany). N,N‐Dimethylformamide (DMF) (HPLC grade, 99.8%), N-methylpyrrolidone (NMP) (anhydrous, > 99% purity), and Lithium chloride (anhydrous, > 99% purity) were purchased from Sigma-Aldrich. Nickel chloride hexahydrate (NiCl₂·6H₂O, 98%), and Ferrous chloride tetrahydrate (FeCl₂·4H₂O, 99.99%) were purchased from Alfa Aesar (Thermo Fisher Scientific, United States). Hydrazine hydrate reducing agent (N₂H₄·H₂O, 99%) was obtained from Fisher (Horsham, UK). Sodium hydroxide (NaOH, 98%) catalyst was purchased from Trading Dynamic co. TDC (Cairo, Egypt). Distilled water was used as a solvent for nanostructured alloys syntheses. Figure 1 illustrates the chemical structure of PES polymer.Figure 1

The structure of poly(ethersulfone) (PES) polymer.

Nady N., Salem N, & Kandil S.H. (2022). Novel magnetic iron–nickel/poly(ethersulfone) mixed matrix membranes for oxygen separation potential without applying an external magnetic field. Scientific Reports, 12, 13675.

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