Opitical rotations were measured on an Autopol VI (Serial #91058) manufactured by Rudolph Research Analytical, Hackettstown, NJ, USA. UV spectra were recorded by a Shimadzu UV-2401PC spectrometer. CD spectra were recorded using a JASCO J-810 spectropolarimeter. NMR spectra were recorded on Bruker Avance III 600 spectrometers. Electrospray ionization (ESI)-high-resolution mass spectrometry (HRMS) were recorded on an Agilent G6230 TOF spectrometer. Single crystal X-ray crystallography was determined on SMART APEX II DUO X-ray single crystal diffractometer using Cu Kα radiation. Preparative HPLC was performed on a Waters 2489 series instrument with a UV/Visible detector, using a reversed-phase C18 column (Phenomenex, 250 mm × 21.2 mm, 5 μm). Chiral HPLC was carried out on an Agilent 1260 liquid chromatograph, utilizing chiral analytical columns [(R, R) WHELK-01 column, 4.6 mm × 250 mm, 10 μm, 100 A].
G6230 tof spectrometer
Manufactured by Agilent Technologies
The G6230 TOF spectrometer is a high-performance time-of-flight mass spectrometer designed for analytical applications. It measures the mass-to-charge ratio of ions in a sample, providing information about the molecular composition of the sample.
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Lab products found in correlation
Avance 3 600 spectrometer, by Bruker (2 mentions)
Uv 2401pc spectrometer, by Shimadzu (1 mentions)
Autopol 6, by Rudolph Research Analytical (1 mentions)
1260 liquid chromatograph, by Agilent Technologies (1 mentions)
2 489 series instrument, by Phenomenex (1 mentions)
J 810 spectropolarimeter, by Jasco (1 mentions)
1100 liquid chromatograph, by Agilent Technologies (1 mentions)
Sepa 300 polarimeter, by Horiba (1 mentions)
Tensor 27 ftir spectrometer, by Bruker (1 mentions)
Silica gel 60 f254, by Qingdao Marine Chemical (1 mentions)
2 protocols using g6230 tof spectrometer
1
Characterization of Organic Compounds
2
Spectroscopic Analysis of Organic Compounds
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Optical rotations were recorded on a Horiba SEPA-300 polarimeter. UV spectra were acquired on a Shimadzu UV-2401A instrument. IR spectra were collected on Bruker Tensor 27 FTIR spectrometers with KBr pellets. NMR spectra were recorded on Bruker Avance III-600 spectrometers with tetramethylsilane as an internal standard at room temperature. HRTOF-ESIMS were recorded on an Agilent G6230 TOF spectrometer. TLC was performed on precoated TLC plates (200-250 µm thickness, silica gel 60 F 254 , Qingdao Marine Chemical Inc.), and the spots were visualized by heating after spraying with 10 % aqueous H 2 SO 4 . Semi-preparative HPLC was performed on an Agilent 1100 liquid chromatograph with a Zorbax SB-C18 (5 µm, 9.4 mm × 250 mm, 3 mL/min) column.
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