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2 protocols using 4 chloropyridine hydrochloride

1

Synthesis of Pyridine Derivatives

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Reagents were purchased from the following vendors and used as received. Tellurium oxide (TeO2): Alfa Aesar, hydroiodic acid: BTC chemical, pyridine, 4-chloropyridine hydrochloride, 4-bromopyridine hydrochloride, 4-iodopyridine, pyrazine: Sigma Aldrich.
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2

Synthesis and Characterization of Organic Compounds

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Sodium hydrogen carbonate, sodium sulfate (Na2SO4) and 6N hydrochloric acid (HCl) were purchased from Scharlau; sodium hydroxide (NaOH) from Merck, 4-methylpyridine, 1,3bis(bromomethyl)benzene, 1-decanol, 1-octadecanol, 4-chloropyridine hydrochloride, hydrogen peroxide (H2O2), sodium borohydride (NaBH4), hydrogen tetrachloroaurate (III) (HAuCl4), sodium citrate tribasic dihydrate, potassium bromide (KBr), ibuprofen, piroxicam, tetraoctylammonium bromide, phosphate buffered saline (PBS) pH=7.4 and 5.2 were purchased from Sigma-Aldrich. Metallic sodium and ammonia 20 % were purchased from Panreac and hexa(ethylene glycol)alkyl thiol (HS-C11-(EG)6-OH) was purchased from Prochimia. Acetonitrile (MeCN), dichloromethane (CH2Cl2), methanol (MeOH), diethyl ether (Et2O), chloroform (CHCl3), ethanol (EtOH), dimethyl sulfoxide (DMSO), tetrahydrofuran (THF), dimethylformamide (DMF), toluene, dimethylsulfoxide-d6 (CD3)2SO and chloroform-d (CDCl3) were purchased from Sigma-Aldrich.
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