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3 protocols using sodium trifluoroacetate

1

Synthesis of Gold Nanoparticles

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Hydrogen tetrachloroaurate(III) tetrahydrate (99.9%), hydrazine monohydrate (98.0%), sodium trifluoroacetate (97.0%), methanol (99.7%), tetrahydrofuran (99.5%) (THF), Irganox1010, polyethylene glycol 400 (PEG400), D(+)-glucose (98.0%), and meropenem sodium carbonate (>99.5%) were purchased from FUJIFILM Wako Pure Chemical Industries, Ltd. MPyCA (98.0%) and CHCA (99.0%) were purchased from Sigma Aldrich. The water used in this study was purified by a water distillation apparatus (water distillation apparatus, Aquarius RFD250, ADVANTEC).
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2

Sensitive MALDI-TOF MS Analysis

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BPA, trifluoroacetic acid (TFA), LC/MS grade acetonitrile (ACN), polyethylene glycol (PEG) 200 and PEG600, sodium trifluoroacetate (TFANa) were purchased from FUJIFILM Wako Pure Chemical Corporation (Osaka, Japan). 2,5-Dihydroxybenzoic acid (DHB) and α-Cyano-4-hydroxycinnamic acid (CHCA) was purchased from Tokyo Chemical Industry Co., Ltd. (Tokyo, Japan).
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3

Polymer Characterization by HPLC

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Reagents PEO (average molecular weight (Mw) = 2000, Shodex, Tokyo, Japan), PPO (Mw = 2000, Wako, Osaka, Japan), poly(EO-r-PO) (Mw = 2500, EO unit 70 wt%, Sigma-Aldrich, St. Louis, MO), PEO-b-PPO-b-PEO (Mw = 2000, EO unit 10 wt%, Sigma-Aldrich), and PPO-b-PEO-b-PPO (Mw = 2000, EO unit 50 wt%, Sigma-Aldrich) were used as analytes. The polymers were dissolved (0.1 mg/mL each) in a mixture of acetonitrile/water (50/50, v/v) containing 0.01% sodium trifluoroacetate (Wako).
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