Methanol (MeOH; LC gradient grade), acetonitrile (ACN; LC gradient grade), and glacial acetic acid (HAc; MS grade) were purchased from Merck (Darmstadt, Germany). Mycotoxin standards were purchased from Romer Labs Diagnostic GmbH Tulln, Austria, including: nivalenol (NIV), 13 C-NIV, DON, 13 C-DON, deepoxy-DON (DOM-1), OTA, 13 C-OTA, AFM 1 , 13 C-AFM 1 , citrinin (CIT), FB 1 , 13 C-FB 1 , 13 C-ZEN or Sigma, Vienna, Austria (ZEN, α-and β-zearalenol (ZEL)). The deuterated [ 2 H 4 ] alternariol (AOH) was synthesized by [31] (link) and kindly provided by Prof. Michael Rychlik, TU Munich. Solid standard substances were dissolved in pure ACN (α-and β-ZEL; [ 2 H 4 ] AOH). All other standards were delivered in either ACN or ACN/H 2 O (FB 1 ) and stored at -20 °C. A combined multi-standard working solution for preparation of calibrants and spiking experiments was prepared in ACN, and also, fresh mixture of 13 C and deuterated [ 2 H 4 ] stable isotope standards were prepared as described by [32] .
Citrinin
Manufactured by Romer Labs
Sourced in United States, Austria
Citrinin is a piece of lab equipment designed for the detection and quantification of the mycotoxin citrinin in various food and feed samples. It operates based on high-performance liquid chromatography (HPLC) technology to provide accurate and reliable results.
Automatically generated - may contain errors
Lab products found in correlation
Acetonitrile, by Merck Group (2 mentions)
Ochratoxin a, by Romer Labs (2 mentions)
Nivalenol, by Romer Labs (1 mentions)
13c don, by Romer Labs (1 mentions)
Afm 1, by Romer Labs (1 mentions)
Cysteine, by Merck Group (1 mentions)
Deoxynivalenol, by Romer Labs (1 mentions)
Zearalenone, by Romer Labs (1 mentions)
Chloroauric acid, by Merck Group (1 mentions)
15 acetyldeoxynivalenol, by Romer Labs (1 mentions)
3 acetyldeoxynivalenol, by Romer Labs (1 mentions)
β zearalanol β zal, by Romer Labs (1 mentions)
Milli q water, by Merck Group (1 mentions)
Hexane, by Merck Group (1 mentions)
Acetone, by Merck Group (1 mentions)
Ammonium acetate, by Merck Group (1 mentions)
Formic acid, by Merck Group (1 mentions)
Ms grade formic acid, by Thermo Fisher Scientific (1 mentions)
Hplc grade ethanol, by Merck Group (1 mentions)
Milli q system, by Merck Group (1 mentions)
3 protocols using citrinin
1
Simultaneous Mycotoxin Quantification Protocol
2
Comprehensive Analysis of Mycotoxins in Chinese Grains
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AFB1, AFB2, AFG1, AFG2, AFM1, AFM2, ochratoxin A (OTA), ochratoxin α (OTα), deoxynivalenol (DON), 3-acetyldeoxynivalenol (3-ADON), 15-acetyldeoxynivalenol (15-ADON), neosolaniol (NEO), fusarenon X (Fus X), citrinin (CIT), fumonisins B1 (FB1), fumonisins B2 (FB2), zearalenone (ZEN), zearalanone(ZAN), α-zearalenol (α-ZOL), β-zearalenol (β-ZOL), α-zearalanol (α-ZAL), and β-zearalanol (β-ZAL) were purchased from Romer Labs, Inc. (Union, MO, USA). Sterigmatocystin (STM), gliotoxin (GLI), cyclopiazonic acid (CPA), patulin (PAT), alternariol (AOH), alternariolmethyether (AME) and altenuisin (ALS) were purchased from Sigma-Aldrich (St. Louis, MO, USA). Acetonitrile, hexane, acetone, formic acid, chloroauric acid, cysteine and ammonium acetate were also obtained from Sigma-Aldrich. Milli-Q water (Millipore, Billerica, MA, USA) was used for all analyses.
A total of 40 samples, including 20 peanut samples, 10 wheat samples, and 10 maize samples, were purchased from bazaars in Shanghai, China.
A total of 40 samples, including 20 peanut samples, 10 wheat samples, and 10 maize samples, were purchased from bazaars in Shanghai, China.
3
Mycotoxin and Monacolin Quantification
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Citrinin (solution in acetonitrile 100 μg mL−1), ochratoxin A (solution in acetonitrile 100 μg mL−1) and aflatoxin mix containing AFB1 and AFB2 (2 μg mL−1 in acetonitrile), AFG1 and AFG2 (0.5 μg mL−1 in acetonitrile) were obtained from Romer Labs (Tulln, Austria). Monacolin K (25 mg), monacolin K acid (5 mg) and simvastatin (10 mg) were purchased from Vinci Biochem S.R.L. (Florence, Italy).
HPLC-grade ethanol, and acetonitrile were purchased from Sigma-Aldrich (Taufkirchen, Germany); bidistilled water was obtained using Milli-Q System (Millipore, Bedford, MA, USA). MS-grade formic acid from Fisher Chemical (Thermo Fisher Scientific Inc., San Jose, CA, USA) was also used.
HPLC-grade ethanol, and acetonitrile were purchased from Sigma-Aldrich (Taufkirchen, Germany); bidistilled water was obtained using Milli-Q System (Millipore, Bedford, MA, USA). MS-grade formic acid from Fisher Chemical (Thermo Fisher Scientific Inc., San Jose, CA, USA) was also used.
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