1 butanethiol

Manufactured by Merck Group

Sourced in United States

1-butanethiol is a clear, volatile liquid organic compound with the chemical formula CH3(CH2)3SH. It is primarily used as a chemical intermediate in the synthesis of other organic compounds. Its core function is to serve as a versatile reagent in various chemical reactions and processes.

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Butanethiol (2 citations)

6 protocols using 1 butanethiol

Synthesis and Characterization of Imprinted Polymers

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HTM (1), l-histidine (HTD, 2), imidazole (IDZ, 3),
and tryptamine (TTM, 4) were purchased from Sigma-Aldrich
and used as received. Methacrylic acid (MAA, 5) and ethylene
glycol dimethacrylate (EGDMA, 6) were purchased from
Sigma-Aldrich and purified by passing through basic alumina (Al₂O₃) columns. AIBN was obtained from Sigma-Aldrich
and recrystallized in ethanol twice before use. Carbon disulfide and
1-butanethiol (both from Sigma-Aldrich) were used as received. MCEBTTC
(7) was synthesized according to the procedure outlined
below. High-performance liquid chromatography (HPLC)-grade solvents,
such as dimethyl sulfoxide (DMSO) (Sigma-Aldrich), acetonitrile (MeCN)
(Honeywell Burdick & Jackson), and methanol (Fisher Scientific),
were used without further purification. Na₂HPO₄ (BDH Chemicals), NaH₂PO₄·2H₂O (AJAX Chemicals), KH₂PO₄ (Sigma-Aldrich),
and H₃PO₄ (85%) (Sigma-Aldrich) were used as received
(Figure 1).

Romano EF J.r., So R.C., Donne S.W, & Holdsworth C.I. (2016). Preparation and Binding Evaluation of Histamine-Imprinted Microspheres via Conventional Thermal and RAFT-Mediated Free-Radical Polymerization. ACS Omega, 1(4), 518-531.

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Radiolabeled Branched PEI Nanoparticle Synthesis

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PEI (Branched, Mw = 25,000), chloramine-T trihydrate (ch-T), HPAO, 1-butanethiol, potassium iodide (KI), acetic anhydride (Ac₂O), triethylamine (TEA), phosphate buffered saline (PBS), and 1-ethyl-3-(3-(dimethylamino)propyl) carbodiimide hydrochloride (EDC) were supplied by Sigma-Aldrich (St. Louis, MO). PEG monomethyl ether with one end terminating in a carboxyl group (mPEG-COOH, Mw = 5000), PEG with one end terminating in a maleimide group and the other in a succinimidyl valerate group (MAL-PEG-SVA, Mw = 5000), and cellulose dialysis membranes were obtained from Shanghai Yanyi Biotechnology Corporation (Shanghai, China). CTX peptide was manufactured by Shanghai Bootech BioScience & Technology Co., Ltd. (Shanghai, China). Na¹³¹I solution was obtained from Shanghai GMS Pharmaceutical Co., Ltd. (Shanghai, China). Disposable PD-10 desalting columns, fluorescein isothiocyanate (FI), cell counting kit-8 (CCK-8), C6 glioma cells, fetal bovine serum (FBS), RPMI 1640 medium, penicillin, and streptomycin were procured from Shanghai Dobio CO., Ltd. (Shanghai, China). HAuCl₄·4H₂O, sodium borohydride (NaBH₄), and all other chemicals and solvents were supplied by Sinopharm Chemical Reagent Co., Ltd. (Shanghai, China).

Zhao L., Li Y., Zhu J., Sun N., Song N., Xing Y., Huang H, & Zhao J. (2019). Chlorotoxin peptide-functionalized polyethylenimine-entrapped gold nanoparticles for glioma SPECT/CT imaging and radionuclide therapy. Journal of Nanobiotechnology, 17, 30.

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Synthesis of Chalcogenide Nanocrystals

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1-Octadecene
(90%), oleic acid (90%), CdO
(≥99.99%), Se powder (100 mesh, 99.99%), trichloroethylene
(anhydrous, ≥ 99%), 1-butanethiol (99%), 1-pentanethiol (98%),
1-hexanethiol (97%), 1-heptanethiol (98%), 1-octanethiol (≥98.5%),
1-nonanethiol (98%), 1-decanethiol (96%), 2-methyl-1-butanethiol (99%),
3-methyl-1-butanethiol (97%), 2-ethyl-1-hexanethiol (97%), 2-methyl-1-hexanoic
acid (98%), 5-methyl-1-hexanoic acid (98%), 4-methyl-1-octanoic acid
(98%), 4-ethyl-1-octanoic acid (98%), 4-methyl-1-nonanoic acid (99%),
LiAlH₄, p-toluenesulfonyl chloride (99%),
thiourea (99%), toluene-d₈ (99.6% D),
and chloroform-d₁ (99.8% D) were purchased
from Sigma-Aldrich, Alfa Aesar, or Acros Organics.

Elimelech O., Aviv O., Oded M., Peng X., Harries D, & Banin U. (2022). Entropy of Branching Out: Linear versus Branched Alkylthiols Ligands on CdSe Nanocrystals. ACS Nano, 16(3), 4308-4321.

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Comprehensive Analysis of Sulfur Compounds

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The studied sulfur compounds: ethanethiol (97%), dimethyl sulfide (99%), 1-propanethiol (99%), thiophene (99%), diethyl sulfide (98%), 1-butanethiol (99%), dimethyl disulfide (99%), ethyl thioacetate (98%), 1-pentanethiol (98%), 2-(methylthio)ethanol (99%), 3-(methylthio)propionaldehyde (96%), dipropyl sulfide (97%), diethyl disulfide (99%), thiophenol (97%), 2-methyltetrahydrothiophene-3-one (97%), 3-thiophenecarboxaldehyde (98%), 3-(methylthio)-1-propanol (98%), 2-thiophenecarboxaldehyde (98%), ethyl 3-(methylthio)propionate (99%), dibutyl sulfide (98%), dipropyl disulfide (98%), and benzothiazole (96%) were purchased from Sigma-Aldrich (St. Louis, MO, USA). Ethanol and sodium chloride were obtained from Chempur (Piekary Slaskie, Poland). EDTA was purchased from Sigma-Aldrich (St. Louis, MO, USA). Distilled water was purified with use of Millipore Simplicity UV purification system (18.2 MΩ·cm, Simplicity Millipore Waters, Milford, MA, USA).

Dziekońska-Kubczak U., Pielech-Przybylska K., Patelski P, & Balcerek M. (2020). Development of the Method for Determination of Volatile Sulfur Compounds (VSCs) in Fruit Brandy with the Use of HS–SPME/GC–MS. Molecules, 25(5), 1232.

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Synthesis of Functional Nanomaterials via RAFT Polymerization

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Poly(ethylene glycol) methyl ether acrylate (PEGA, average Mn = 480 g mol -1 ), n-butyl acrylate (n-BA, >99%) and t-butyl acrylate (t-BA 98%), Bromo-propionic acid (>99%), 1butanethiol (99%), carbon disulphide (>99%) and tannic acid (ACS reagent) were obtained from Sigma-Aldrich. All monomers above were passed through basic aluminium oxide to remove inhibitor before use. Chloroform-d3 (99.8% D atom), was obtained from Sigma Aldrich and used for 1 H NMR spectroscopy. Thermal initiator 4,4′-azobis(4-cyanovaleric acid) (ACVA, >98%, Aldrich), was used as received. Cyanine 7.5 amine was purchased from Lumiprobe. TEM grids were purchased from EM Resolutions Ltd (Sheffield, UK). RAFT agent, 2-(((butylthio)carbonothioyl)thio)propanoic acid (PABTC) was synthesised as previously described. 22

Gurnani P., Sanchez-Cano C., Abraham K., Xandri-Monje H., Cook A.B., Hartlieb M., Lévi F., Dallmann R, & Perrier S. (2018). RAFT Emulsion Polymerization as a Platform to Generate Well-Defined Biocompatible Latex Nanoparticles. Macromolecular bioscience, 18(10).

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Synthesis of Heterogeneous Catalysts

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All the organic reagents were commercial products of analytical purity and were used without further purication. The silica and carbon based heterogeneous catalysts were obtained from Johnson Matthey (5% Pt/SiO 2 Batch M04483, JM ref.
108070; 5% Ru/SiO 2 Batch M04484, JM ref. 108070; 5% Ru/C Batch M02070, JM ref. 94890). The 5% Pt/OMS-2 (cryptomelane-type manganese oxide) was prepared as reported previously. 41 1-Butanethiol (99%) and thiophenol ($99%) were purchased from Sigma-Aldrich.

Pavel O.D., Podolean I., Parvulescu V.I., Taylor S.F.R., Manyar H.G., Ralphs K., Goodrich P, & Hardacre C. (2018). Impact of SCILL catalysts for the S-S coupling of thiols to disulfides. Faraday discussions, 206.

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