The prewetted carbon nonwoven (10 × 10 mm2) was placed in a round-bottom flask and treated with 25 mL of 1 M HCl, and then the mixture was heated to 80 °C. After reaching the required temperature, isoamyl nitrite (0.7 mL, 5 mmol) and 4-bromoaniline (0.86 g, 5 mmol) (Sigma-Aldrich, Poznan, Poland) were added to the mixture. The reaction was carried out at 80 °C for 18 h. Finally, the nonwoven fabric was washed with DMF (3 × 5 mL) and DCM (3 × 5 mL).
Isoamyl nitrite
Manufactured by Merck Group
Sourced in Poland
Isoamyl nitrite is a clear, colorless liquid chemical compound used in certain research and laboratory applications. It has a characteristic fruity odor. The core function of isoamyl nitrite is as a reagent in organic synthesis reactions.
Automatically generated - may contain errors
6 protocols using isoamyl nitrite
1
Functionalization of Carbon Nonwoven
2
Functionalization of Carbon Nonwoven Fabric
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The following materials were used for the reaction: 10 × 10 mm2 prewetted carbon nonwoven fabric, 25 mL of 1 M HCl, isoamyl nitrite (0.7 mL, 5 mmol), and 4-aminophenol (0.55 g, 5 mmol) (Sigma-Aldrich, Poznan, Poland). The reaction was carried out at 80 °C for 18 h. The modified CF-1e nonwoven was washed with DMF (3 × 5 mL) and DCM (3 × 5 mL).
3
Functionalization of Carbon Nonwoven Fabric
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The following materials were used for the reaction: 10 × 10 mm2 prewetted carbon nonwoven fabric, 25 mL of 1 M HCl, isoamyl nitrite (0.7 mL, 5 mmol), and 1,4-diaminobenzene (0.54 g, 5 mmol) (Sigma-Aldrich, Poznan, Poland). The reaction was carried out at 80 °C for 18 h. The modified CF-1d nonwoven was washed with DMF (3 × 5 mL) and DCM (3 × 5 mL).
4
Functionalization of Carbon Nonwoven Fabric
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A carbon nonwoven (CF ) of size 10 × 10 mm2 was wetted by treating with 15 mL DMF (J.T. Baker Avantor Performance Materials, Gliwice, Poland) for 5 min. Then the nonwoven was treated with a mixture of DMF: 1 M HCl (15 mL) (1:1) for 5 min and 1 M HCl (15 mL) for 10 min. Next, nonwoven fabric was transferred to a round-bottom flask and treated with 25 mL of 1 M HCl and heated to 80 °C. The reaction mixture was stirred gently. After reaching the required temperature, isoamyl nitrite (0.7 mL, 5 mmol) (Sigma-Aldrich, Poznan, Poland) and aniline derivative (5 mmol) were added to the solution. The reaction was conducted at 80 °C for 18 h. Finally, the nonwoven was washed with DMF (3 × 5 mL) and DCM (3 × 5 mL).
5
Functionalization of Carbon Nonwoven
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The following materials were used for the reaction: 10 × 10 mm2 prewetted carbon nonwoven fabric, 25 mL of 1 M HCl, isoamyl nitrite (0.7 mL, 5 mmol), and 4-aminobenzoic acid (0.71 g, 5 mmol) (Sigma-Aldrich, Poznan, Poland). The reaction was carried out at 80 °C for 18 h. The modified CF-1c nonwoven was washed with DMF (3 × 5 mL) and DCM (3 × 5 mL).
6
Azo Dye Synthesis on Carbon Fabric
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The following materials were used for the reaction: 10 × 10 mm2 prewetted carbon nonwoven fabric, 25 mL of 1 M HCl, isoamyl nitrite (0.7 mL, 5 mmol), and 4-chloroaniline (0.64 g, 5 mmol) (Sigma-Aldrich, Poznan, Poland). The reaction was carried out at 80 °C for 18 h. The modified CF-1b nonwoven was washed with DMF (3 × 5 mL) and DCM (3 × 5 mL).
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