2400c elemental analyzer

Manufactured by PerkinElmer

The 2400C Elemental Analyzer is a laboratory instrument designed to perform accurate and reliable analysis of the elemental composition of a wide range of samples. It utilizes combustion technology to determine the carbon, hydrogen, nitrogen, and sulfur (CHNS) content of organic and inorganic materials.

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Lab products found in correlation

Spectrum 100 ftir spectrophotometer, by PerkinElmer (2 mentions) Mercury vx 400 spectrometer, by Agilent Technologies (2 mentions) V 570 spectrometer, by Jasco (2 mentions) Rf 5301pc luminescence spectrophotometer, by Shimadzu (1 mentions) Spectrometers, by Agilent Technologies (1 mentions) Rf 5301pc fluorescence spectrophotometer, by Shimadzu (1 mentions) Equinox 55 spectrometer, by Bruker (1 mentions)

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Elemental analyzer (9 citations)

5 protocols using 2400c elemental analyzer

Characterization of Organic Compounds

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All chemicals
used for the experimental research were of reagent grade. The melting
points were measured using a Boetius block device. A PerkinElmer spectra
100 FT-IR spectrophotometer was applied for the analysis of the infrared
spectra. A Varian spectrometer was applied for ¹H NMR and ¹³C NMR spectra. A PerkinElmer 2400C elemental analyzer was
applied to carry out elemental analyses. The luminescence spectra
were measured, applying a Shimadzu RF-5301PC luminescence spectrophotometer.
A VG ZAB-HS mass spectrometer was applied to measure the mass spectra.

Zhao Z.X., Wu Y.Y., Zhao D.X, & Liu Q.X. (2023). Preparation of a Tetra-Imidazolium Salt and Sensing for p-Dinitrobenzene. ACS Omega, 8(7), 6869-6874.

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Comprehensive Characterization Methods

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Total commercially available chemicals for synthesis and test were of reagent grade. A Boetius Block apparatus was used for the report of melting points. A PerkinElmer Spectrum 100 FT-IR spectrophotometer was used for the report of Infrared (IR) spectra. A Varian spectrometers was used for the report of ¹H NMR and ¹³C NMR spectra. The measurement of the elemental analyses was carried out on a Perkin-Elmer 2400C Elemental Analyzer. Ultraviolet spectra were recorded on a PerkinElmer Lamber35 UV spectrophotometer. The fluorescence spectra were carried out in a Shimadzu RF-5301PC fluorescence spectrophotometer. A VG ZAB-HS mass spectrometer was used to record EI mass spectra.

Liu Y., Zhao Z., Huo R, & Liu Q. (2019). Two macrocycle-based sensors for anions sensing. Scientific Reports, 9, 502.

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Synthesis and Characterization of Substituted Benzenes

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1,4-Bis(bromomethyl)-2,3,5,6-tetramethylbenzene^{23 (link)} and N-R-benzimidazole^{24 (link)} were prepared according to the methods in literature.
The solvents were purified according to the standard procedures, and
Schlenk techniques were used in all manipulations. All commercially
available chemicals in the experiments were of reagent grade and used
as received. A Boetius Block apparatus was used to determine the melting
points of products. A Varian Mercury Vx 400 spectrometer was used
to record ¹H and ¹³C NMR spectra at 400 and
100 MHz, respectively. Chemical shifts, δ, were reported in
parts per million (ppm) for both ¹H and ¹³C
NMR. Coupling constant (J) values were given in hertz
(Hz). The elemental analyses were carried out on a PerkinElmer 2400C
Elemental Analyzer. A Focus DSQI GC–MS was used, which was
equipped with an integrator (C-R8A) with a capillary column (CBP-1
or CBP-5, 0.25 mm i.d. × 40 m).

Liu Q.X., Hu Z.L., Yu S.C., Zhao Z.X., Wei D.C, & Li H.L. (2018). NHC Pd(II) and Ag(I) Complexes: Synthesis, Structure, and Catalytic Activity in Three Types of C–C Coupling Reactions. ACS Omega, 3(4), 4035-4047.

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Characterization of Organic Compounds

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The solvents and chemicals used for synthesis and analysis were analytical grade and obtained commercially. A RF-5301PC ﬂuorescence spectrophotometer (Shimadzu) was used to record fluorescence spectra at room temperature. The excitation and emission slits were set to 10 nm. UV–vis absorption spectra were recorded at room temperature using a JASCO-V570 spectrometer. A Varian spectrometer was employed to record ¹H and ¹³C NMR spectra. A Perkin-Elmer 2400C Elemental Analyzer was employed for elemental analyses. IR spectra were measured with a PerkinElmer Spectrum 100 FT-IR spectrophotometer. A Q-TOF LC/MS (Agilent) and a VG ZAB-HS (VG) mass spectrometer were applied for HRMS analysis. Melting points were recorded employing a Boetius Block apparatus.

Liu Q.X., Yang F., Zhao Z.X., Yu S.C, & Ding Y. (2019). Preparation of anthracene-based tetraperimidine hexafluorophosphate and selective recognition of chromium(III) ions. Beilstein Journal of Organic Chemistry, 15, 2847-2855.

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Synthesis and Characterization of Imidazole Derivatives

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N-ethyl-imidazole and N-ⁿbutyl-imidazole were prepared according to the methods of literature reported^{67 (link),77 (link)}. Schlenk techniques were used in all manipulations. All the reagents for synthesis and analyses were of analytical grade and used without further purification. Melting points were determined with a Boetius Block apparatus. ¹H and ¹³C NMR spectra were recorded on a Varian Mercury Vx 400 spectrometer at 400 MHz and 100 MHz, respectively. Chemical shifts, δ, are reported in ppm relative to the internal standard TMS for both ¹H and ¹³C NMR. J values are given in Hz. Elemental analyses were measured using a Perkin-Elmer 2400 C Elemental Analyzer. The fluorescence spectra were performed using a Cary Eclipse fluorescence spectrophotometer. UV-vis spectra were recorded on a JASCO-V570 spectrometer. EI mass spectra were recorded on a VG ZAB-HS mass spectrometer (VG, U.K.). IR spectra (KBr) were taken on a Bruker Equinox 55 spectrometer.

Liu Y., Zhao Z, & Liu Q. (2018). Preparation of Macrometallocycle and Selective Sensor for Copper Ion. Scientific Reports, 8, 10943.

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