Cm300 fegtem high resolution transmission electron microscope

Example 5

Morphology of the MOF nanocrystals and hybrid nanofibers were observed under JEOL JSM 6700 field emission scanning electron microscope at an accelerating voltage of 5 kV. All samples were coated with a thin gold layer before SEM imaging.

TEM images were obtained with Philips CM300 FEGTEM high resolution transmission electron microscope.

Wide-angle X-ray diffraction (XRD) measurements were performed using a Bruker D8 Discover GADDS X-ray diffraction meter with Cu Kα radiation and Raman spectra were recorded on Jobin Yvon T64000 triple spectrograph micro-Raman system.

The metal content in the resultant hybrid carbon fibers was measured by inductively coupled plasma mass spectrometry (ICP-MS) analysis.

The specific surface area and pore size analysis was measured using a Micromeritics ASAP 2020 system.

Example 5

Morphology of the MOF particles and hybrid fibrous mats were observed under JEOL JSM 6700 field-emission scanning electron microscope at an accelerating voltage of 5 kV. All samples were coated with a thin gold layer before SEM imaging.

TEM images were obtained with a Philips CM300 FEGTEM high resolution transmission electron microscope.

The specific surface area and pore size analysis was measured using a Micromeritics ASAP 2020 system.

Electrical resistivity of the hybrid carbon fibrous mats was measured using a multimeter.

Example 5

Morphology of the MOF nanocrystals and hybrid nanofibers were observed under JEOL JSM 6700 field emission scanning electron microscope at an accelerating voltage of 5 kV. All samples were coated with a thin gold layer before SEM imaging TEM images were obtained with Philips CM300 FEGTEM high resolution transmission electron microscope.

Wide-angle X-ray diffraction (XRD) measurements were performed using a Bruker D8 Discover GADDS X-ray diffraction meter with Cu Kα radiation and Raman spectra were recorded on Jobin Yvon T64000 triple spectrograph micro-Raman system.

The metal content in the resultant hybrid carbon fibers was measured by inductively coupled plasma mass spectrometry (ICP-MS) analysis.

The specific surface area and pore size analysis was measured using a Micromeritics ASAP 2020 system.