XRD patterns were obtained from GE-XRD 3003 TT with CuKα1 radiation (λ = 1.5406 Å) for 2θ = 5–60°. The UV/VIS data was taken from PerkinElmer UV Lambda 650 UV/VIS spectrometer. The TGA analysis was carried out using NETZSCH STA 2500 instrument. PL spectra was recorded using Horiba/Jobin Yvon FluoroLog-3 Modular Spectrofluorometer. JASCO FT/IR-6600 spectrometer was used to record the Fourier transform infrared spectrum. The AFM instrument in non-contact mode with model number MFP-3D was used to record the images. HRTEM was carried out using FEI-TECNAI G2-20 TWIN 200 kV instrument. The Raman characterization is done using the instrument LABRAM HR-[Horiba-Jobin Yvon]. Horiba Scientific Horiba SZ-100 instrument was utilised to record the particle size from DLS analysis. ZEISS Gemini SEM 300 was used to record the FESEM images and EDX.
Ft ir 6600 spectrometer
Manufactured by Jasco
Sourced in Japan
The FT/IR-6600 spectrometer is a Fourier Transform Infrared (FT-IR) spectrometer designed for analytical applications. It uses infrared radiation to analyze the chemical composition and structure of various materials. The spectrometer measures the absorption or transmission of infrared light by the sample, providing information about the molecular bonds and functional groups present in the material.
Automatically generated - may contain errors
Lab products found in correlation
Geminisem 300, by Zeiss (1 mentions)
Labram hr, by Horiba (1 mentions)
Fluorolog 3 modular spectrofluorometer, by Horiba (1 mentions)
Vertex 70, by Bruker (1 mentions)
Cary 7000, by Agilent Technologies (1 mentions)
P 2000 polarimeter, by Jasco (1 mentions)
Rp c18, by YMC (1 mentions)
Synergi rp c18 column, by Phenomenex (1 mentions)
Avance 3 300, by Bruker (1 mentions)
Chirascan spectropolarimeter, by Applied Photophysics (1 mentions)
V 550 spectrophotometer, by Jasco (1 mentions)
Avance 3 600, by Bruker (1 mentions)
Ultimate 3000 instrument, by Thermo Fisher Scientific (1 mentions)
Agilent 1260 instrument, by Agilent Technologies (1 mentions)
Peg 6000, by Merck Group (1 mentions)
D8 advance x ray diffractometer, by Bruker (1 mentions)
Lcms 2010a system, by Shimadzu (1 mentions)
Ftir 610, by Jasco (1 mentions)
Silica gel 60 f254, by Merck Group (1 mentions)
500 mhz nmr, by Bruker (1 mentions)
10 protocols using ft ir 6600 spectrometer
1
Comprehensive Material Characterization Protocol
2
Characterization of PAAS Photonic Film
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The hemispherical reflectance spectra of the PAAS photonic film were characterized by a spectrophotometer (Agilent Cary 7000) with a polytetrafluoroethylene-based integrating sphere (Model IS200, Thorlabs) over solar wavelengths (0.3–2.5 µm). The hemispherical reflectance spectra were measured by the FTIR spectrometer (Vertex 70) equipped with a golden integrating sphere (A562, Bruker) from 2.5 µm to 15 µm. The Raman spectra were examined by the BSTEK BWS 465 Raman spectrometer from 800 cm−1 to 950 cm−1. The film formation process was observed under a magnification ratio of 15 X utilizing Bruker Hyperion optical microscopy (IHYP 1126). The FTIR transmittance spectra were measured by the Jasco FTIR 6600 spectrometer from 4000 to 500 cm−1.
3
Structural Analysis of Natural Compounds
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Optical rotations were measured with a JASCO P-2000 polarimeter (Jasco, Tokyo, Japan). UV spectra were recorded on a JASCO V-550 spectrophotometer (Jasco, Tokyo, Japan). IR spectra were performed on a FT/IR-6600 spectrometer (Jasco, Tokyo, Japan). NMR spectra were acquired on a Bruker Avance III-600 and a Bruker Avance III-300 instruments (Bruker, Bremerhaven, Germany). High-resolution mass spectra were obtained on a LCQ Advantage MAX (Finnign, USA). CD spectrum was measured on a Chirascan spectropolarimeter (Applied Photophysics, Ltd.). X-ray Crystallography was collected at 100 K on a Rigaku Oxford Diffraction Supernova Dual Source, Cu at Zero equipped with an AtlasS2 CCD using Cu Kα radiation. Silica gel (80−100 and 200−300 mesh, Qingdao Haiyang, Qingdao, China), Sephadex LH-20 (Pharmadex), and RP-C18 (AA12S50, YMC) were used for column chromatography. Preparative HPLC was carried out using an Ultimate 3000 instrument (Thermo Scientific, USA) with a Waters XBridge RP-C18 column (250 mm×10 mm). Analytical HPLC was run on using an Agilent 1260 instrument (Agilent, USA) with a Phenomenex Synergi RP-C18 column (250 mm×4.6 mm).
4
Spectroscopic Characterization of Organic Compounds
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The experiments were conducted using commercially available reagents and solvents without any additional purification. Melting points were measured using a Barnstead electrothermal digital melting point apparatus (model IA9100, BIBBY scientific limited, Staffordshire, UK). IR spectra were recorded using a Jasco FT/IR-6600 spectrometer (Tokyo, Japan). NMR spectra were obtained using a Bruker 700 MHz NMR spectrometry instrument (Zurich, Switzerland). Electrospray ionization (ESI) mass spectrometry (MS) experiments were carried out using an Agilent 6320 ion trap mass spectrometer equipped with an ESI ion source (Agilent Technologies, Palo Alto, CA, USA). High-resolution mass spectrometry was performed using an HRMS JMS 700 JEOL mass spectrometry instrument (Tokyo, Japan). The compounds were judged to be pure based on NMR spectroscopic studies. All spectra for 1H-NMR, 13CNMR and Mass spectra are found in the Supplementary Materials .
5
Synthesis and Characterization of Copper Nanoparticles
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Copper nitrate trihydrate (Cu(NO3)2.3H2O), sodium hydroxide (NaOH), ethanol, ET, poly ethylene glycol (PEG, 6000), and polyvinyl acetate (PVA) were obtained from Merck (Darmstadt, Germany). UV/Vis spectra were recorded through Perkin Elmer (Waltham, MA, USA), UV/Vis spectrometer, Lambda 25. The FT-IR spectrum was performed on a JASCO FT/IR-6600 spectrometer. X-ray diffractometry (XRD) was conducted by using a D8 advance Bruker X-ray diffractometer equipped with a Cu anode (Bruker, Bremen, Germany).
6
Characterization of Rhenium Complexes
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1H NMR spectra were recorded in CDCl3 or CD3CN on a JEOL ECA400-II system at 400 MHz. Transmission IR spectra in CH2Cl2 or the reaction solution were recorded on a JASCO FT/IR-610 or FT/IR-6600 spectrometer at 1 cm–1. Electrospray ionization-mass spectroscopy (ESI-MS) was performed using a Shimadzu LC-MS-2010 A system with MeCN as the mobile phase. Solutions containing 5 mM complexes and 0.1 M Et4NBF4 were prepared for the FT-IR measurements, and a solution containing only 0.1 M Et4NBF4 was used for the background measurements. Ultra high performance chromatograms (UHPLC) of the Re complexes were recorded on a SHIMADZU UHPLC Nexera X2 with an ODS column (Waters Acquity: 150 mm × 2.1 mm i.d.), a Shimadzu DGU-20A degasser, an LC-30AD pump, an SPD-M30A UV-vis photodiode-array detector, and a Rheodyne 7125 injector. The eluent was a 1 : 1 (v/v) mixture of methanol and water containing 0.05 M KH2PO4 (pH 5.9), and the flow rate was 0.2 mL min–1.
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1H NMR spectra were recorded in CDCl3 or CD3CN on a JEOL ECA400-II system at 400 MHz. Transmission IR spectra in CH2Cl2 or the reaction solution were recorded on a JASCO FT/IR-610 or FT/IR-6600 spectrometer at 1 cm–1. Electrospray ionization-mass spectroscopy (ESI-MS) was performed using a Shimadzu LC-MS-2010 A system with MeCN as the mobile phase. Solutions containing 5 mM complexes and 0.1 M Et4NBF4 were prepared for the FT-IR measurements, and a solution containing only 0.1 M Et4NBF4 was used for the background measurements. Ultra high performance chromatograms (UHPLC) of the Re complexes were recorded on a SHIMADZU UHPLC Nexera X2 with an ODS column (Waters Acquity: 150 mm × 2.1 mm i.d.), a Shimadzu DGU-20A degasser, an LC-30AD pump, an SPD-M30A UV-vis photodiode-array detector, and a Rheodyne 7125 injector. The eluent was a 1 : 1 (v/v) mixture of methanol and water containing 0.05 M KH2PO4 (pH 5.9), and the flow rate was 0.2 mL min–1.
7
Characterization of Organic Compounds
8
FTIR Analysis of Extract Functional Groups
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FTIR spectra were acquired using a JASCO FTIR-6600 spectrometer (Japan) to determine the functional groups present in the extracts. Solid samples (1 mg) of each extract were placed on the sample holder of the FTIR spectrophotometer and scanned between 4000 and 400 cm−1 to obtain the spectra that were then interpreted.
9
Synthesis and Characterization of Iridium Hydride Complexes
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All manipulations were performed
with rigorous exclusion of air at an argon/vacuo manifold using standard
Schlenk-tube or glovebox techniques. Solvents were dried by the usual
procedures and distilled under argon prior to use. 1H, 13C{1H}, 31P{1H}, 29Si{1H}, and 19F{1H} NMR spectra
were recorded on a Bruker ARX or Bruker Avance 300 MHz instrument.
Chemical shifts (expressed in parts per million) are referenced to
residual solvent peaks (1H and 13C{1H}) and 85% H3PO4 (31P{1H}). Coupling constants J are given in hertz. Infrared
spectra were recorded on a JASCO FT-IR 6600 spectrometer. [IrH(Cl)(κ2-NSitBu2)(coe)] (1 ) and [IrH(OTf)(κ2-NSitBu2)(coe)] (4 ) were prepared
according to published methodologies.22 (link)
with rigorous exclusion of air at an argon/vacuo manifold using standard
Schlenk-tube or glovebox techniques. Solvents were dried by the usual
procedures and distilled under argon prior to use. 1H, 13C{1H}, 31P{1H}, 29Si{1H}, and 19F{1H} NMR spectra
were recorded on a Bruker ARX or Bruker Avance 300 MHz instrument.
Chemical shifts (expressed in parts per million) are referenced to
residual solvent peaks (1H and 13C{1H}) and 85% H3PO4 (31P{1H}). Coupling constants J are given in hertz. Infrared
spectra were recorded on a JASCO FT-IR 6600 spectrometer. [IrH(Cl)(κ2-NSitBu2)(coe)] (
according to published methodologies.22 (link)
10
Characterization of MGR-Ox-AuNPs@MIP Nanocomposites
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The MGR-Ox-AuNPs@MIP nanocomposites were characterized by scanning electron microscopy (SEM, S-2500, Hitachi High-tech International Trading Co., Ltd., Shanghai, China). Electrochemical measurements were performed on the electrochemical workstation (PGSTAT302N, Netherlands). The FT-IR spectra were recorded by a Jasco FT-IR 6600 spectrometer. The electrochemical impedance spectroscopy (EIS) measurements were performed using a 0.02 M [Fe(CN)6 -3/-4 ] solution (frequency range: 0.1 to 10000 Hz, signal amplitude: 0.01 V). Electrochemical measurements were carried out based on a typical three-electrode system, using a modified CPE as working electrode, platinum electrode as an auxiliary electrode, and Ag/ AgCl, KCl as a reference electrode.
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