7683b series autosampler

Manufactured by Agilent Technologies

The 7683B series autosampler from Agilent Technologies is a precision liquid handling system designed for automated sample injection in analytical instruments. It features a programmable sample tray and injection mechanism to provide consistent and reliable sample introduction.

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Lab products found in correlation

5975c mass spectrometer, by Agilent Technologies (3 mentions) 7890a gc system, by Agilent Technologies (3 mentions) Hp 5ms, by Agilent Technologies (2 mentions) Masshunter workstation software package, by Agilent Technologies (1 mentions) Gc ms system, by Agilent Technologies (1 mentions) 5975c series mass spectrometry, by Agilent Technologies (1 mentions)

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7683B autosampler (12 citations) 7683B series (12 citations)

4 protocols using 7683b series autosampler

GC-MS Analytical Procedure for Compound Identification

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The GC–MS instrument consisted in an Agilent 7890 A GC system equipped with an Agilent 7683B series autosampler and interfaced to a single quadrupole Agilent 5975C mass spectrometer. The column was an Agilent HP-5MS (30 m × 0.25 mm, 0.25 µm film thickness). The gas carrier (He) flow was constant at 1 mL/min. The samples were analysed in full scan mode (adopted libraries: NIST08, WILEY27, SWGDRUG4). The oven temperature was initially set at 100 °C for 2.25 min, programmed to 180 °C at 40 °C/min and to 300 °C at 10 °C/min for 10 min. Injector and transfer line temperatures were always 300 and 230 °C, respectively. The injection volume was 1 mL in splitless mode. Data acquisition and elaboration were performed using the Agilent MassHunter Workstation software package.

Bertol E., Vaiano F., Mari F., Di Milia M.G., Bua S., Supuran C.T, & Carta F. (2017). Advances in new psychoactive substances identification: the U.R.I.To.N. Consortium. Journal of Enzyme Inhibition and Medicinal Chemistry, 32(1), 841-849.

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GC/MS Analysis of ATCA Compounds

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GC/MS analysis was performed on an Agilent GC/MS system, which consists of a 7890A series of gas chromatography, a 5975C series mass spectrometry, and a 7683B series auto-sampler (Agilent, Santa Clara, CA). The column used was a DB-5 bonded phase column (30 m × 0.25 mm × 0.25 μm) with helium as a carrier gas at the flow rate of 1 mL/min. The GC/MS program was adopted from Logue et al. with minor modifications. Briefly, the autosampler was set to inject 1 μL of sample into the injection port, which was held at 290°C and contained a Cyclosplitter liner (Restek, Bellefonte, PA). The total flow was set to be 54 mL/min with the septum purge flow of 3 mL/min and a 10:1 split ratio. Using the described method, the ATCA-(TMS)₃ and the ATCA-¹³C, ¹⁵N-(TMS)₃ were eluted at approximately 8.76 min, with a total run time of 13 min. The ions selected were as follow: ATCA-(TMS)₃ (245, 347, and 362 m/z) and ATCA-¹³C, ¹⁵N-(TMS)₃ (248, 350, and 365 m/z) under selected ion monitoring (SIM) mode. The dwell time was set to 50 ms.

Yi Li S., Petrikovics I, & Yu J.(. (2019). Development of magnetic carbon nanotubes for dispersive micro solid phase extraction of the cyanide metabolite, 2-aminothiazoline-4-carboxylic acid, in biological samples. Journal of chromatography. B, Analytical technologies in the biomedical and life sciences, 1109, 67-75.

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GC-MS Analysis of Organic Compounds

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The GC–MS system consisted of an Agilent 7890A GC system equipped with an Agilent 7683B series autosampler and interfaced via an electronic impact source to a single quadrupole Agilent 5975C mass spectrometer. Helium was used as a gas carrier at a 1 mL/min constant flow. The GC-MS methodology was the same used in previous studies [13 (link)].

Argo A., Zerbo S., Buscemi R., Trignano C., Bertol E., Albano G.D, & Vaiano F. (2022). A Forensic Diagnostic Algorithm for Drug-Related Deaths: A Case Series. Toxics, 10(4), 152.

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GC-MS Analysis of Organic Compounds

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The GC-MS instrument consisted of an Agilent 7890A GC system equipped with an Agilent 7683B series autosampler and interfaced via electronic impact source to a single quadrupole Agilent 5975C mass spectrometer. The column was an Agilent HP-5MS (30 m Â 0.25 mm, 0.25 mm). Helium was used as gas carrier at constant flow 1 mL/min. Acquisition was in full scan mode in the m/z range 50-550 and identification was by exploiting the NIST08, WILEY27, SWGDRUG4 libraries. The oven program was: initial isotherm 100 C for 2.25 min, 40 C/min to 180 C and 10 C/min to 300 C, final isotherm 300 C for 10 min Injector and transfer line temperatures were 300 and 230 C, respectively. The injection volume was 1 mL in splitless mode. Data acquisition and elaboration were performed using the ChemStation Workstation software.

Bertol E., Bigagli L., D'Errico S., D'Errico S., Mari F., Palumbo D., Pascali J.P, & Vaiano F. (2018). Analysis of illicit drugs seized in the Province of Florence from 2006 to 2016. Forensic science international, 284.

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