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1 4 butanediol dimethacrylate

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1,4-butanediol dimethacrylate is a chemical compound used in the manufacturing of various lab equipment. It serves as a crosslinking agent, playing a core function in the formation of polymeric materials.

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Lab products found in correlation

Tert butylbenzene, by Merck Group (1 mentions) Urethane dimethacrylate monomer, by Merck Group (1 mentions) Blocbuilder ma, by Arkema (1 mentions) Hydroxypropyl methacrylate, by Merck Group (1 mentions) 2 hydroxy 2 methylpropiophenone, by Merck Group (1 mentions) Avs titrinorm, by Avantor (1 mentions) Butyl acrylate, by Merck Group (1 mentions) Srcl2, by Merck Group (1 mentions) Pegmem, by Merck Group (1 mentions) Zncl2, by Merck Group (1 mentions) Thiazolyl blue tetrazolium bromide mtt, by Merck Group (1 mentions) Alizarin red s, by Merck Group (1 mentions) Ammonium persulfate, by Merck Group (1 mentions) Acetic acid, by Merck Group (1 mentions) Glutaraldehyde, by Merck Group (1 mentions)

3 protocols using 1 4 butanediol dimethacrylate

1

Preparation and Characterization of Mix-MA Monomer Benchmark

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The blend “Mix-MA”, used as
a benchmark monomer, has been prepared with 33.3 wt % of (hydroxypropyl)methacrylate,
33.3 wt % of 1,4-butanediol dimethacrylate, and 33.3 wt % of a urethane
dimethacrylate monomer, obtained from Sigma Aldrich and represented
in Scheme 2. Mix-MA
was already used in previous works.3 (link),4 (link) More particularly,
its viscosity is well adapted for the preparation of formulations.
In addition, interestingly, Mix-MA is not too viscous. Therefore,
oxygen inhibition occurs, and only good-performance systems can polymerize
it. BlocBuilder-MA was obtained from Arkema. tert-Butylbenzene was obtained from Sigma-Aldrich.
Bonardi A.H., Dumur F., Gigmes D., Xu Y.Y, & Lalevée J. (2020). Light-Induced Thermal Decomposition of Alkoxyamines upon Infrared CO2 Laser: Toward Spatially Controlled Polymerization of Methacrylates in Laser Write Experiments. ACS Omega, 5(6), 3043-3046.
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2

Synthesis of Carboxylated Nanodiamond Composites

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The monomers, butyl acrylate (BA; 99%, Sigma-Aldrich, Helsinki, Finland) and N,N-dimethylaminoethyl methacrylate (DMAEMA; 99%, Acros Organics/VWR, Vantaa, Finland), as well as the cross-linker, 1,4-Butanediol dimethacrylate (BuDMA; 95%, Sigma-Aldrich, Helsinki, Finland), were distilled under reduced pressure, and were run through an anhydrous alumina column and a filter to remove the inhibitors and oligomers. The photoinitiator, 2-hydroxy-2-methylpropiophenone (97%, Sigma-Aldrich, Helsinki, Finland), carboxylated detonation nanodiamond powder (μDiamond® Molto Vox; Carbodeon Oy, Vantaa, Finland), and acetonitrile (ACN; 99.9%, Sigma-Aldrich, Helsinki, Finland) were used as received. Deionized ultrapure water with ~18 mΩ/cm resistivity was used as received from the purifier. Carbonate buffer (AVS Titrinorm; VWR, Helsinki, Finland) was used as received.
Tiainen T., Lobanova M., Karjalainen E., Tenhu H, & Hietala S. (2020). Stimuli-Responsive Nanodiamond–Polyelectrolyte Composite Films. Polymers, 12(3), 507.
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3

Antibacterial Hydrogel for Bone Regeneration

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PEGMEM [poly(ethylene glycol) methyl ether methacrylate] with average Mn = 300, DEM [2-(dimethylamino)ethyl methacrylate], 1,4-butanediol dimethacrylate, ammonium persulfate (APS), ZnCl2, SrCl2, glutaraldehyde, acetic acid, Thiazolyl Blue Tetrazolium Bromide (MTT), and Alizarin Red S were purchased from Sigma-Aldrich. α-Tricalcium-phosphate (α-TCP) was purchased from Fluka.
Simulated body fluid (SBF) solution was prepared according to British Standard ISO 23317:200.
Gram-positive bacteria, methicillin-resistant Staphylococcus aureus (MRSA)—MRSA (NCTC 12493) and Staphylococcus epidermidis (RP62a), were used. Bacteria frozen stocks were stored at −80°C; weekly, strains were streaked out on Brain Heart Infusion (BHI) plates (Oxoid) and incubated for 24 h at 37°C and then stored at 4°C.
Tommasi G., Perni S, & Prokopovich P. (2016). An Injectable Hydrogel as Bone Graft Material with Added Antimicrobial Properties. Tissue Engineering. Part A, 22(11-12), 862-872.
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