The starting materials RhCl3·3H2O, IrCl3·3H2O, 2-phenylpyridine, 8-aminoquinoline, 1-napthylamine and 1-methyl-2-imidazolecarboxaldehyde were purchased from Sigma–Aldrich and used without further purification. All the solvents were dried by usual methods prior to use. The cyclometalated iridium(III) and rhodium(III) chloro bridged dimer [Ir(ppy)2Cl]2 and [Rh(ppy)2Cl]2 was prepared according to the literature methods [74 –75 ].
8 aminoquinoline
Manufactured by Merck Group
Sourced in United Kingdom
8-aminoquinoline is a chemical compound used as a laboratory reagent. It is a white to off-white crystalline solid. 8-aminoquinoline is commonly used for various analytical and research applications in chemistry and biochemistry laboratories.
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Lab products found in correlation
2 phenylpyridine, by Merck Group (1 mentions)
Potassium carbonate, by Thermo Fisher Scientific (1 mentions)
Diethyl ether, by Avantor (1 mentions)
Ethanethiol, by Merck Group (1 mentions)
Dimethylformamide, by Avantor (1 mentions)
Sodium hydroxide (naoh), by Thermo Fisher Scientific (1 mentions)
2 hydroxyethyl disulfide, by Merck Group (1 mentions)
Aldrithiol 2, by Merck Group (1 mentions)
1 methylpiperazine, by Merck Group (1 mentions)
4 bromo 1 8 naphthalic anhydride, by Merck Group (1 mentions)
N n dimethylethylendiamine, by Merck Group (1 mentions)
N hexane, by Avantor (1 mentions)
Ethanol, by Merck Group (1 mentions)
2 mercaptoethanol, by Merck Group (1 mentions)
Triethylamine, by Merck Group (1 mentions)
Cysteamine hydrochloride, by Merck Group (1 mentions)
2 protocols using 8 aminoquinoline
1
Synthesis of Cyclometalated Iridium and Rhodium Complexes
2
Synthesis of Naphthalic Anhydride Derivatives
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4-Bromo-1,8-naphthalic anhydride, FA, ethanethiol, cysteamine hydrochloride, 2-mercaptoethanol, aldrithiol-2, 1-methylpiperazine, N,N-dimethylethylendiamine, 8-aminoquinoline, 2-hydroxyethyl disulfide, tris(2-carboxyethyl)phospine hydrochloride, potassium hydroxyde and triethylamine were purchased from Sigma-Aldrich (UK); ethanol, methanol, dichloromethane ethyl, acetate, acetone, acetonitrile and the low iron silica sand were purchased from Fluka (UK). Diethyl ether, n-hexane, dimethylformamide, tetrahydrofurane (HPLC grade) and the silica gel were purchased by VWR. Potassium carbonate was provided by Alfa Aeser (UK). Ultra-dry dimethyl sulfoxyde 99.7% and sodium hydroxide were obtained by Fisher scientific (UK). 2-Methoxyethanol from Honeywell Riedel-de Haen (UK). Chloroform-D and dimethyl sulfoxide-D6 by Cambridge Laboratories (UK). All the reagents were used without further purification.
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