The structural characterizations of the SF-BGE, TA, and SF-BGE/TA solutions and the SF-BGE/TA/ZnO hydrogel were conducted by attenuated total reflectance-Fourier transform infrared spectroscopy (ATR-FTIR; ALPHA-P, Bruker, Billerica, MA, USA). The spectrum was obtained in the spectral range of 4000–400 cm−1 with a resolution of 4 cm−1. Each sample was freeze-dried and measured in the solid state.
Alpha p
Manufactured by Bruker
Sourced in Germany, United States, Italy
The Alpha-P is a laboratory instrument designed for the analysis of materials. It provides accurate measurements of physical and chemical properties, such as particle size, zeta potential, and molecular weight. The Alpha-P utilizes advanced technology to deliver reliable and consistent results, making it a valuable tool for scientific research and industrial applications.
Automatically generated - may contain errors
Lab products found in correlation
Opus software, by Bruker (3 mentions)
Dsc n 650, by Scinco (2 mentions)
D8 advance, by Bruker (2 mentions)
Asap 2020, by Micromeritics (2 mentions)
Icap rq, by Thermo Fisher Scientific (2 mentions)
Ultima 4 with cu kα radiation, by Rigaku (2 mentions)
Mira3 feg, by TESCAN (2 mentions)
Originpro 9, by OriginLab (2 mentions)
Nova230, by Thermo Fisher Scientific (1 mentions)
D max 2500, by Rigaku (1 mentions)
Tristar 3000, by Micromeritics (1 mentions)
Cf400 cu 50, by Electron Microscopy Sciences (1 mentions)
Elexsys 500, by Bruker (1 mentions)
Smartlab se, by Rigaku (1 mentions)
Microtof 2, by Bruker (1 mentions)
Smartlab x ray diffractometer, by Rigaku (1 mentions)
Escalab xi instrument, by Thermo Fisher Scientific (1 mentions)
Jem 2100, by JEOL (1 mentions)
Optima 8300 dv, by PerkinElmer (1 mentions)
Zetasizer nano z, by Malvern Panalytical (1 mentions)
42 protocols using alpha p
1
ATR-FTIR Characterization of SF-BGE/TA Hydrogel
2
Infrared Spectral Analysis of Burned Paper
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Infrared spectra of the various areas of the burned paper depending on the extent of the burning were obtained using FT-IR – ATR (Attenuated Total Reflection) (Bruker alpha-P, diamond ATR crystal, Germany). Spectral collection was performed under ambient conditions with the following operating conditions: range 4000-400 cm−1; resolution 4 cm−1; scan number 128.
3
Confirmation of Silica Nanoparticle Bonding by FT-IR
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
Example 13
Fourier-Transform Infrared Spectroscopy (FT-IR)
Confirmation of bonding between silica nanoparticles and different azole units via different functional groups was done by FT-IR spectroscopy. Determination of the existence of functional groups in molecules was also conducted by comparing the experimental FT-IR absorbance or transmission peaks with databases. When new fillers are introduced to a composite, FT-IR is a valuable method in evaluating the functional groups that bind the fillers with polymer matrix. Many studies were conducted in literature to understand bonding between functionalized fillers and resin matrix. All samples were dried under vacuum and stored in a glove box before FT-IR analysis. FT-IR spectra with the range of 4000-400 cm−1 and a resolution of 4 cm−1 were recorded with an ATR system of Bruker Alpha-P.
4
ATR-FTIR Analysis of Dry Composites
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The dry composites obtained in step 1 of the fabrication of the scaffolds were analyzed by ATR–FTIR to confirm the complete evaporation of the solvent, DMF. A Bruker Alpha-P FTIR spectrometer was used in the absorbance mode, with ATR platinum–diamond coupling. The dry composites were analyzed at RT, with a spectral resolution of 4 cm−1 at 64 scans per sample, and in the range 4000–400 cm−1.
5
FTIR Characterization of Biosynthesized SPIONs
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
FTIR measurement was performed to confirm the functional groups of biosynthesized SPIONs by Fourier transform infrared spectrometer (Bruker, Germany, Alpha-P). The SPIONs suspension was dropped on the sample holder. The spectrum absorbance of samples was recorded in the range of 4000–400 cm−1 at a resolution of 4 cm-1.
6
Multimodal Characterization of Nanomaterials
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The samples were characterized by using X-ray diffraction (XRD, Rigaku D/Max-2500(SWXD) and Rigaku D/Max-RB (12 KW)) using Cu Kα radiation (λ = 0.15406 nm), scanning electron microscopy (SEM, FEI Nova230), a transmission electron microscope (TEM, Philips Technai F20), Raman spectroscopy (Horiba Jobin Yvon ARAMIS) using Ar ion CW Laser (514.5 nm), X-Ray photoelectron spectroscopy (XPS, Thermo VG Scientific Sigma Probe), and Fourier-transform infrared spectroscopy (FT-IR, Bruker Alpha-P). N2-sorption was carried out at 77 K by a Tristar 3000, Micromeritics (U.S.A).
7
Comprehensive Characterization of Nanocrystals
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
All measurements were collected at room-temperature unless specified otherwise. Electronic absorption spectra were collected on colloidal suspensions in air-tight quartz cuvettes with 1 cm pathlengths (Cary 50 Bio). EPR spectra were measured at X-band frequency (9.6 GHz) with a Bruker Elexsys-500 equipped with a Super High QE (ER4123SHQE) cavity. Transmission electron microscopy (TEM) images of NCs deposited onto copper grids (CF400-CU-50, Electron Microscopy Sciences) with a 3 nm carbon coating (JEOL TEM-2000FX). Powder X-ray diffraction patterns were collected in the Bragg–Brentano configuration with a Cu Kα source (Rigaku SmartLab SE). FTIR spectra were collected using Bruker Alpha-P equipped with a diamond attenuated total reflectance (ATR) crystal. High resolution electrospray ionization mass spectra (ESI-MS) were collected in negative ion mode with Bruker MicroTOF-II. In a typical sample preparation for ESI-MS, the aqueous reaction mixture from the hydrothermal synthesis was centrifuged to separate NCs from the rest of the water-soluble side-products. The aqueous supernatant was used for ESI-MS measurements with no further purification.
8
Characterization of Citrate-Stabilized Gold
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
For the investigation of citrate stabilization and gold formation, the samples were characterized with Fourier transform infrared spectroscopy. Potassium bromide pellets containing 1% (wt/wt) of sample were analyzed using a FTIR spectrometer (Alpha-P, Bruker, Billerica, MA, USA). OPUS software (Bruker, Billerica, USA) was used for background subtraction and baseline correction.
9
FTIR Analysis of Piper betle Extract
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The FTIR Spectrometer (Alpha P; Bruker, Germany) was used, which was interlinked to desktop operated Windows system to connect with OPUS Data Collection software (Version 7.5; Bruker, Germany). Prior to the analysis, the attenuated total reflectance (ATR) plate was cleaned thoroughly by using ethanol (70%), after which it was dried with a soft tissue. For loading the sample, one drop of P. betle extract was placed onto the crystal of the ATR plate, while keeping the anvil arm in upright position by active rotation. The FTIR spectra were obtained with the addition of 100 scans in the range of 4000–400 cm−1 at a resolution of 4 cm−1 [97 (link)].
10
Measuring Orthodontic Adhesive Degree of Cure
Check if the same lab product or an alternative is used in the 5 most similar protocols
+ Expand
The orthodontic adhesives (n=3) were placed on the attenuated total reflectance device of a Fourier transformed infrared (FTIR) spectrometer (Alpha-P; Bruker Optics, Ettlingen, Germany). Each sample was photoactivated for 40 s using the light-emitting diode. The photoactivation was standardized at 1 mm between the light-unit tip and the samples. The same light-curing unit, irradiance, and radiometer were used for all subsequent methodologies. Spectra from FTIR analysis were recorded before and 1 minute after photoactivating each sample with 32 scans and a 4 cm−1 resolution. The DC was estimated based on the area of the 1638 cm−1 peak (carbon-carbon double bonds of aliphatic chain) and 1608 cm−1 peak (carbon-carbon double bonds of aromatic chain) using the following formula:
About PubCompare
Our mission is to provide scientists with the largest repository of trustworthy protocols and intelligent analytical tools, thereby offering them extensive information to design robust protocols aimed at minimizing the risk of failures.
We believe that the most crucial aspect is to grant scientists access to a wide range of reliable sources and new useful tools that surpass human capabilities.
However, we trust in allowing scientists to determine how to construct their own protocols based on this information, as they are the experts in their field.
Ready to get started?
Sign up for free.
Registration takes 20 seconds.
Available from any computer
No download required
Revolutionizing how scientists
search and build protocols!