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2 protocols using 4 ethylphenol

1

Characterization of Phenolic Compounds

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Phenol (99%, GC), 4-ethylPhenol (99%, GC), 4-propylPhenol (99%, GC), 4-methylguaiacol (98%, GC), 4-allylguaiacol (99%, GC), syringol (98%, GC) and 4-methylsyringol (98%, GC) were purchased from Tokyo Chemical Industry Co., (TCI). Guaiacol (99%, GC), 4-ethylguaiacol (>98%) were purchased from Adamas. SBA-15 was purchased from XFNANO. All these chemicals obtained from commercial resources were used directly.
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2

Aroma and Flavan-3-ols Standards Characterization

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Aroma standards including phenylethyl alcohol, linalool, rose oxide, β-damascenone, geraniol, nerol, α-terpineol, β-citronellol, ethyl butanoate, ethyl hexanoate, ethyl octanoate, ethyl decanoate, ethyl cinnamate, isoamyl acetate, ethyl 3-methylbutanoate, eugenol, whiskey lactone, 4-ethylphenol, guaiacol and 3-octanol with purity ≥97% were purchased from Tokyo Chemical Industry (Shanghai, China). Flavan-3-ols standards including (+)-catechin, (−)-epicatechin, (−)-epicatechin-3-O-gallate, (−)-epigallocatechin with purity higher than 98% were supplied by Sigma-Aldrich (St. Louis, MO, USA). Folin-Ciocalteau reagent, p-dimethylamino-cinnamaldehyde (DMACA), dimethylsulfoxide (DMSO‑d6 containing 0.03% tetramethylsilane) were supplied from Merck (Darmstadt, Germany). All reagents of analytical grade were provided by Kermel (Tianjin, China), and all solvents of chromatographic grade were from Oceanpak (Gothenburg, Sweden).
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