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Benzoyl bromide

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Benzoyl bromide is a laboratory reagent used as a precursor in organic synthesis. It is a colorless to pale yellow liquid with a pungent odor. Benzoyl bromide serves as an acylating agent, introducing a benzoyl group to various organic compounds.

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Lab products found in correlation

Oleic acid, by Merck Group (5 mentions) Cesium carbonate, by Merck Group (5 mentions) Oleylamine, by Merck Group (4 mentions) Toluene, by Merck Group (3 mentions) Ethyl acetate, by Thermo Fisher Scientific (2 mentions) 1 octadecene, by Merck Group (2 mentions) Lead 2 acetate trihydrate, by Merck Group (2 mentions) Benzoyl chloride, by Merck Group (2 mentions) Ethyl acetate, by Merck Group (2 mentions) Octadecene, by Merck Group (2 mentions) Lead acetate trihydrate, by Merck Group (2 mentions) Didodecyldimethylammonium bromide, by Merck Group (2 mentions) Dodecane, by Merck Group (1 mentions) Tetrachloroethylene, by Merck Group (1 mentions) Lead thiocyanate, by Merck Group (1 mentions) Lead bromide, by Merck Group (1 mentions) Copper 2 chloride dihydrate, by Merck Group (1 mentions) Hexane, by Merck Group (1 mentions) Hydrochloric acid (hcl), by Merck Group (1 mentions) Acetone, by Merck Group (1 mentions)

5 protocols using benzoyl bromide

1

Synthesis of Lead Halide Perovskites

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Lead bromide (PbBr2, ≥98%),
lead thiocyanate (Pb(SCN)2, 99.5%), cesium carbonate (Cs2CO3, 99%), oleylamine (OLAM, 70%), oleic acid (OA,
90%), 1-octadecene (ODE, 90%), tetrachloroethylene, toluene (anhydrous,
99.8%), lead(II) acetate trihydrate (≥99.5%), benzoyl bromide
(97%), and dodecane were purchased from Sigma-Aldrich. Cesium acetate
(99%) and ethyl acetate (≥99.5%) were purchased from Fisher
Scientific. All chemicals were used without further purification;
lead compounds were stored inside a nitrogen-filled glovebox.
Toso S., Baranov D., Altamura D., Scattarella F., Dahl J., Wang X., Marras S., Alivisatos A.P., Singer A., Giannini C, & Manna L. (2021). Multilayer Diffraction Reveals That Colloidal Superlattices Approach the Structural Perfection of Single Crystals. ACS Nano, 15(4), 6243-6256.
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2

Synthesis of Colloidal Metal Nanocrystals

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Cesium carbonate (Cs2CO3, 99.9%), silver acetate (Ag(OAc), 99%),
indium(III) acetate (In(OAc)3, 99.99% trace metal basis), copper(II) acetate
(Cu(OAc)2, 99.99% trace metal basis), cesium chloride (CsCl, 99.9%), silver
chloride (AgCl, 99.999% trace metal basis), indium(III) chloride (InCl3,
99.999% trace metal basis), copper(II) chloride dihydrate
(CuCl2·2H2O, 99.0%), oleic acid (OA, 90%), oleylamine (OAm,
70%), benzoyl bromide (Bz-Br, 97%), benzoyl chloride (Bz-Cl, 99%), diphenyl ether (DPE,
99%), hydrochloric acid (HCl, 37%), hexane (anhydrous, 95%), acetone (99.5%), and
2-propanol (99.5%) were obtained from Sigma-Aldrich. All chemicals were used as received
without further purification.
Kim K., Kim H, & Park J. (2021). Bandgap Modulation of Cs2AgInX6 (X = Cl and Br) Double Perovskite Nano- and Microcrystals via Cu2+ Doping. ACS Omega, 6(41), 26952-26958.
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3

Cesium-lead Halide Nanocrystal Synthesis

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Cesium carbonate (Cs2CO3, 99.9%), lead (II) acetate trihydrate (Pb(OAc)2 · 3H2O, 99.999%), benzoyl chloride (99%), benzoyl bromide (97%), and iodotrimethylsilane (97%), oleic acid (OA, technical grade, 90%), oleylamine (OAm, technical grade, 70%), 1-octadecene (ODE, technical grade, 90%) were purchased from Sigma-Aldrich. Toluene, hexanes, and ethyl acetate were purchased from Fisher Scientific. All chemicals were used as received without further purification.
Yi J., Ge X., Liu E., Cai T., Zhao C., Wen S., Sanabria H., Chen O., Rao A.M, & Gao J. (2020). The correlation between phase transition and photoluminescence properties of CsPbX3 (X = Cl, Br, I) perovskite nanocrystals. Nanoscale Advances, 2(10), 4390-4394.
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4

Synthesis of Perovskite Nanocrystals

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Cadmium acetate dihydrate ((CdAc2·2H2O), 99.99%), lead acetate trihydrate ((PbAc2·3H2O), 99.99%), cesium carbonate (Cs2CO3, reagent Plus, 99%), benzoyl bromide (C6H5COBr, 97%), ethyl acetate (98.8%), toluene (anhydrous,
99.5%), phenethylammonium bromide (≥98%), didodecyldimethylammonium
bromide (DDABr), octadecene (ODE, technical grade, 90%), dimethyl sulfoxide-d6 (DMSO, 99 atom % D) toluene-d8 (99 atom % D), and oleic acid (OA,
90%) were purchased from Sigma-Aldrich. Indium tin oxide (ITO)-patterned
substrates, polystyrene sulfonate (PEDOT:PSS, AL 4083), poly(N,N9-bis(4-butylphenyl)-N,N9-bis(phenyl)-benzidine) (poly-TPD), and 2,2′,2″-(1,3,5-benzinetriyl)-tris(1-phenyl-1-H-benzimidazole) (TPBi) were purchased from Ossila Ltd.
Poly(9-vinylcarbazole) (PVK) and LiF were purchased from Sigma-Aldrich.
Didodecylamine (97%) was purchased from TCI. oleic acid was dried
at 120 °C for an hour and stored in a nitrogen-filled glove box.
All other chemicals were used without further purification.
Imran M., Ramade J., Di Stasio F., De Franco M., Buha J., Van Aert S., Goldoni L., Lauciello S., Prato M., Infante I., Bals S, & Manna L. (2020). Alloy CsCdxPb1–xBr3 Perovskite Nanocrystals: The Role of Surface Passivation in Preserving Composition and Blue Emission. Chemistry of Materials, 32(24), 10641-10652.
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5

Colloidal Nanoparticle Synthesis Protocol

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Lead acetate trihydrate ((PbAc2·3H2O),
99.99%), cesium carbonate (Cs2CO3, reagent Plus,
99%), benzoyl bromide (C6H5COBr, 97%), ethyl
acetate (98.8%), toluene (anhydrous,
99.5%), didodecyldimethylammonium bromide (DDDMAB), oleylamine (70%),
octadecene (ODE, technical grade, 90%), and oleic acid (OA, 90%) were
purchased from Sigma-Aldrich. Didodecylamine (DDDAm, 97%) was purchased
from TCI. All chemicals were used without any further purification.
Palei M., Imran M., Biffi G., Manna L., Di Stasio F, & Krahne R. (2020). Robustness to High Temperatures of Al2O3-Coated CsPbBr3 Nanocrystal Thin Films with High-Photoluminescence Quantum Yield for Light Emission. ACS Applied Nano Materials, 3(8), 8167-8175.
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