Industrial-grade isobutyl alcohol polyoxyethylene ether (IPEG) with a molecular weight of 2400 (average polymerization degree: ~54), and 2-(acryloyloxy) ethyl phosphate (MOEP) and 5-hydroxypentyl prop-2-enoate phosphate (HPEP), were manufactured by Liaoning Kelong Fine Chemical Company (Liaoyang, Liaoning Province, China), and Guangzhou Kinde Chemical Materials Company (Guangzhou, Guangdong Province, China), respectively. Analytical grade acrylic acid (AA), 2-(Dimethylamino)ethyl methacrylate (DMAEMA), Maleic anhydride (MA), N,N′-Methylenebisacrylamide (MBA), potassium persulfate (KPS), mercapto acetic acid (TGA), CaSO4·2H2O, KOH, K2SO4, Na2SO4, and ascorbic acid (VC) were from Sinopharm Chemical Company (Shanghai, China). The schematic drawings of the unsaturated phosphate monomers are exhibited in Figure 1. The phosphate monoester, phosphate diester, and free phosphoric acid of unsaturated phosphate ester are shown in Table 1.
Ordinary Portland cement classified as P Ⅱ 52.5 was purchased from Sichuan E-Sheng Cement Group Co., Ltd. Chemical (Emei, Sichuan Province, China) compositions of cement are tabulated in Table 2.
Chen J., Yang C., He Y., Wang F, & Zeng C. (2024). Effects and Mechanism of Hyperbranched Phosphate Polycarboxylate Superplasticizers on Reducing Viscosity of Cement Paste. Materials, 17(8), 1896.