The hydrogen release reaction of LiCa(AlH4)3 was studied by thermogravimetry (TG, Rigaku TG-8210) with an Al sample holder heated up to 673 K at 5 K/min in a He gas flow of 150 ml/min.
Tg 8210
Manufactured by Rigaku
Sourced in Japan
The TG-8210 is a thermogravimetric analyzer (TGA) manufactured by Rigaku. The TG-8210 is designed to measure the change in mass of a sample as a function of temperature or time in a controlled atmosphere. This instrument is commonly used for thermal analysis applications.
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2 protocols using tg 8210
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Hydrogen Release Kinetics of LiCa(AlH4)3
2
Detailed Characterization of Prepared Samples
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The morphologies of the prepared samples were monitored using a SU1510 instrument (SEM, Hitachi High Technologies Co., Japan). Thermogravimetry-differential thermal analysis (TG-DTA) was conducted using a TG8210 instrument (Rigaku, Japan). The surface area, including the pore volume, was measured using a NOVA4200e instrument (Shimadzu, Japan). Finally, the surface functional groups and point of zero charge (pHpzc) were investigated according to previously reported methods [13 ,14 (link)].
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