The background subtraction and the peak deconvolution for the XPS spectra were performed using the SpecSurf, which is the original analysis software of the JPS‐9010TRX (JEOL) spectrometer. The other statistical tests in this study were performed using igor PRO (WaveMetrics).
Specsurf
Manufactured by JEOL
SpecSurf is a versatile laboratory equipment designed for surface analysis. It utilizes advanced spectroscopic techniques to characterize the physical and chemical properties of material surfaces with high precision and accuracy. The core function of SpecSurf is to provide detailed information about the composition, structure, and behavior of a wide range of materials at the surface level.
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2 protocols using specsurf
1
XPS Spectra Analysis Techniques
2
Comprehensive Characterization of P/AB Powder
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The P/AB powder was characterized by XRD and Raman spectroscopy. The XRD patterns were obtained using a Rigaku SmartLab diffractometer (Cu Kα (λ = 1.5418 Å) and 40 kV-30 mA) equipped with a Si strip high-speed detector (D-teX Ultra 250, Rigaku) under a Bragg-Brentano geometry at the scan rate of 0.5 deg min -1 . The Raman spectra were obtained using a DXR3 Smart Raman (Thermo Fisher Scientific) equipped with a 532 nm diode-pumped solid-state laser at the resolution of 2 cm -1 . The particle size measurement and morphology observation were performed by SEM (Hitachi, SU-8020) and the elemental composition was evaluated by EDX (Horiba EMAXEvolution X-max). The XPS analysis of the P/AB pristine powder was carried out using a JEOL JPS-9010 XPS instrument (MgKα (λ = 9.89 Å), 10 kV-10 mA) with Ar etching at the ion energy of 400 eV for 5 and 10 s. The obtained spectra were analyzed using analytical software (SpecSurf, ver. 1.8.3.7, JEOL, Ltd).
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