Ethyl acetate, methanol, chloroform, toluene, and n-hexane were purchased from Kanto Chemical Co., Tokyo, Japan. Tin(II) octylate, 1-methylimidazole, and tributyl phosphate were obtained from Tokyo Chemical Industry Co., Tokyo, Japan. l -lactide was purchased from Musashino Chemical Laboratory Ltd, Tokyo, Japan.
1 methylimidazole
Manufactured by Tokyo Chemical Industry
Sourced in Japan
1-methylimidazole is a colorless to pale yellow liquid organic compound. It is commonly used as a chemical building block and solvent in various industrial and research applications.
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2 protocols using 1 methylimidazole
1
Synthesis of Polylactide Polymers
2
Synthesis of Compound No. 1
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Example 1
1-Methylimidazole (Tokyo Chemical Industry Co., Ltd.) (5.07 mmol), 11-iodoundecanoic acid (6.09 mmol), and tetrahydrofuran (6 g) were placed in a reaction flask and were reacted by heating under reflux for 3 hours. Then, hexane was added to the reaction flask, and the precipitated crystals were filtered to obtain 1.33 g of a white solid (yield: 67%). It was verified by 1H-NMR and IR that the obtained solid was Compound No. 1. Data are shown in Tables 1 to 3.
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