Thermogravimetric analysis (TGA) of the mycosynthesized AgNPs was conducted in nitrogen atmosphere on a thermogravimetric analyzer (TGA50, Shimadzu Company, Japan). For that, 5 mg of AgNPs were placed in an aluminum pan (Shimadzu Company, Japan; Catalog number: 201–52943) of TGA and the sample was heated in a temperature range of 25–595 °C at a heat rate of 10 °C/min to determine the weight loss profile and the amount of fungal residue on the AgNPs through thermal degradation. The data was analyzed using the TA-60 software (Shimadzu Company, Japan).
Ta 60
Manufactured by Shimadzu
Sourced in Japan
The TA-60 is a thermal analysis instrument manufactured by Shimadzu. It is designed to measure the physical and chemical properties of materials as a function of temperature or time. The TA-60 can be used to perform various thermal analysis techniques, such as thermogravimetric analysis (TGA) and differential scanning calorimetry (DSC).
Automatically generated - may contain errors
Lab products found in correlation
Dsc 60, by Shimadzu (4 mentions)
Tga 50, by Shimadzu (2 mentions)
Tga 60, by Shimadzu (1 mentions)
S 4800 microscope, by Hitachi (1 mentions)
Axis nova, by Shimadzu (1 mentions)
D2 phaser x ray diffractometer, by Bruker (1 mentions)
K alpha, by Thermo Fisher Scientific (1 mentions)
D8 advance, by Bruker (1 mentions)
Adda 2, by Philips (1 mentions)
26 protocols using ta 60
1
Thermal Characterization of Mycosynthesized AgNPs
2
Thermal Stability Analysis by TGA
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Dry samples were tested in aluminum pans in a TGA-50 from Shimadzu (Kyoto, Japan). For this, samples were heated from room temperature to 600 °C at a rate of 10 °C/min under a nitrogen atmosphere and the data was processed with TA60 software version 2.11 from Shimadzu.
3
Thermal Analysis of FLM-Lactose Mixtures
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A DSC-60, Shimadzu differential scanning calorimeter (Kyoto, Japan), with TA-60 software (version 1.51) was used for thermal analysis of FLM and lactose alone, or in binary mixture. Binary mixture (was prepared ( FLM- lactose 1:1 (W/W)), and blended uniformly by tumbling method. Then, DSC pans containing mentioned samples were prepared . and scanned in the temperature range of 25–300°C, with different heating rates (2.5, 10 and 15 °C/min).
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A DSC-60, Shimadzu differential scanning calorimeter (Kyoto, Japan), with TA-60 software (version 1.51) was used for thermal analysis of FLM and lactose alone, or in binary mixture. Binary mixture (was prepared ( FLM- lactose 1:1 (W/W)), and blended uniformly by tumbling method. Then, DSC pans containing mentioned samples were prepared . and scanned in the temperature range of 25–300°C, with different heating rates (2.5, 10 and 15 °C/min).
4
Thermal Characterization of Zeolite-Chitosan Films
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Differential scanning calorimetry (DSC) and termogravimetric analysis (TGA) studies were performed on zeolite-chitosan composite films. TGA was done with a TGA-60 (Shimadzu, Kyoto, Japan) analyzer. All analyses were performed with 10~15 mg samples in platinum pans in a dynamic nitrogen atmosphere (100 mL/min), between 30 °C and 700 °C (10 °C/min). DSC analysis was performed with a DSC-60 (Shimadzu, Kyoto, Japan) analyzer. Samples (approximately 2–3.5 mg) were scanned in a sealed aluminum pan and heated to 550 °C (10 °C/min) under the nitrogen atmosphere (50 mL/min). The weight loss (TGA) and the enthalpies (DSC) were calculated using the TA.60 software provided by Shimadzu.
5
Thermal Analysis of Fine Powder
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The instrument used was DSC-60 (Shimadzu Corp, Japan) with Thermal Analyzer and Operating software of TA 60. The Flow controller was FCL 60. Indium was used as a reference. 5 mg fine powder was used as a sample and was placed in Al pan which was used as the sample holder. It was heated at the rate of 5 °C/min under a Nitrogen atmosphere in the Scanning range of 0–200 °C.
6
Thermogravimetric Analysis of PL-based Composites
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The thermogravimetric analysis (TGA) of the ε-PL, D1821, Na+-Mt, PL-Mt, OMt and PL-OMt was performed on a Shimadzu TA-60 (Kyoto, Japan). Approximately 5 to 10 mg of the sample was heated in a platinum crucible from 30 to 600 or 800 °C at a heating rate of 10 °C/min in a high-purity nitrogen flow of 50 mL/min.
7
Differential Scanning Calorimetry Analysis
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DSC was performed on a TA-60 (Shimadzu, Kyoto, Japan) after being calibrated using indium as the reference material. A sample of 2.0 mg was packed in a hermetically crimped aluminum pan and heated under dry nitrogen flow at 30 mL·min−1. The samples were heated from 25 to 200 °C at a rate of 5 °C min−1.
8
Aceclofenac Crystallinity and Melting Point
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For crystallinity, the samples were evaluated using P-XRD (Panalytical, X’pert), by scanning detector over 2θ angles at a scan rate of 0.01°. The melting point of aceclofenac raw drug, AC-N and fabricated tablet batch were performed by DSC (TA-60, Shimadzu). All the samples, which were about 3 mg, were placed in pans made of aluminum for heating, under 50 mL per min nitrogen flow rate and the scanning was kept at 10°C per min, from 40–200°C.
9
Thermal Analysis of Materials by DSC
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Differential scanning calorimetry (DSC) was performed on a Shimadzu TA-60 (Kyoto, Japan) calorimeter, using 5 mg samples in crimped aluminium pans. The instrument was calibrated using indium and zinc as standards. Nitrogen was used as a purge gas and an empty aluminium pan was used as a reference. Each sample was scanned at a rate of 5°C/min from 25 to 350°C, under N2 atmosphere (flow rate 30 mL/min).
10
Thermal Analysis of Raw and Processed AC
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The melting point and heat of fusion of unprocessed/raw and processed AC was determined by using DSC calorimeter (TA-60, Shimadzu, Japan). In aluminum pans, samples were heated, under nitrogen flow rate (50 mL/min), keeping the rate of scanning 10°C/min from 40°C to 200°C.
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