1 bromoethyl benzene

Manufactured by Merck Group

(1-Bromoethyl)benzene is an organic compound with the chemical formula C6H5CH2CH2Br. It is a colorless liquid used as a laboratory reagent.

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Lab products found in correlation

Cucl2, by Merck Group (1 mentions) Cubr2, by Merck Group (1 mentions) Pmdeta, by Merck Group (1 mentions) Styrene, by Junsei (1 mentions) Na2co3, by Merck Group (1 mentions) Triethylamine, by Merck Group (1 mentions) 2 butanone, by Merck Group (1 mentions) 1 3 5 trioxane, by Merck Group (1 mentions) Carbon disulphide, by Merck Group (1 mentions)

2 protocols using 1 bromoethyl benzene

Purification of Monomers and Catalysts for Polymerization

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Butyl acrylate (TCI, 99%), methyl methacrylate (DAEJUNG CHEMICALS & METALS, Siheung, Korea 99.5%), and styrene (Junsei, Tokyo, Japan, 99.5%) were purified by passing through a basic alumina column before use. Copper(I) bromide (CuBr, Sigma-Aldrich, Seoul, Korea, 98.0%) and copper(I) chloride (CuCl, Sigma-Aldrich, 98.0%) were purified by stirring with glacial acetic acid, followed by filtering and washing the resulting solid four times with ethanol. The solid was dried under a vacuum for two days. Anisole (DAEJUNG CHEMICALS & METALS, 98.0%), (1-Bromoethyl)benzene (Sigma-Aldrich, 98%), copper(II) bromide (CuBr2, Sigma-Aldrich, 98.0%), copper(II) chloride (CuCl2, Sigma-Aldrich, 98.0%) and N,N,N

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-pentamethyldiethylenetriamine (PMDETA, Sigma-Aldrich, 98%), and all other chemicals, internal standards, and solvents were used as received.

Lee S.I., Seo M.G., Huh J, & Paik H.J. (2022). Small-Angle X-ray Scattering Analysis on the Estimation of Interaction Parameter of Poly(n-butyl acrylate)-b-poly(methyl methacrylate). Polymers, 14(24), 5567.

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Synthesis of Polymers via RAFT Polymerization

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Maleic anhydride (MAnh) briquettes (99%, Sigma-Aldrich) and 2,2ʹ-azobis(2-butyronitrile) (AIBN) were purified via recrystallization from toluene and methanol respectively and were dried under vacuum overnight. 2,4,4-Trimethyl-1-pentene (diisobutylene, DIB) (99%, Sigma-Aldrich); 2-butanone (≥99%, Sigma-Aldrich), Na2CO3 (98%, Merck), 1,3,5-trioxane (≥99%, Sigma-Aldrich), 1-butanethiol (97%, Fluka), carbon disulphide (99%, Sigma-Aldrich), triethylamine (99%, Sigma-Aldrich), 1bromoethylbenzene (97%. Sigma-Aldrich), CDCl3 (99.9%, MagniSolv) and acetone-d6 (99.9%, MagniSolv) were used as received. Chloroform was distilled prior to use. The RAFT agent S-butyl-S'-(1-phenyl ethyl) trithiocarbonate (BPT) was synthesized as described in literature. 15

Ball L.E., Riley L.J., Hadasha W., Pfukwa R., Smith C.J.I., Dafforn T.R, & Klumperman B. (2021). Influence of DIBMA Polymer Length on Lipid Nanodisc Formation and Membrane Protein Extraction. Biomacromolecules, 22(2).

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