Raman spectra were acquired using a Horiba LabRAM HR 3D confocal microscope configured with 633 nm (8.5 mW at the sample) and 785 nm (110 mW at the sample) laser lines. A back-illuminated EMCCD (Andor, DU970P) was used for 633-nm experiments and a back-illuminated, deep-depletion CCD (Horiba Synapse) was used for 785-nm experiments. Unless noted otherwise, 633-nm laser excitation was used for Raman measurements. Spectra were acquired with a spectral resolution of 10 cm−1. UV/vis absorption spectra were acquired with a Cary 5G spectrophotometer. Dynamic light scattering and ζ -potential measurements were acquired with a Malvern Zetasizer Nano ZS. Transmission electron microscopy was performed using a JEOL 2100 Cryo transmission electron microscope with an accelerating voltage of 200 kV.
5g spectrophotometer
Manufactured by Agilent Technologies
The 5G spectrophotometer is a laboratory instrument designed to measure the absorbance or transmittance of light in a sample. It operates at frequencies associated with 5G technology. The core function of the 5G spectrophotometer is to analyze the interaction between light and a sample, providing quantitative data about the sample's composition or properties.
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2 protocols using 5g spectrophotometer
1
Raman Spectroscopy and Nanoparticle Characterization
2
Characterization of Perovskite Thin Films
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XRD patterns of the powders and thin films were recorded on a Philips X'PERT diffractometer that was equipped with a proportional detector and a secondary graphite monochromator. The data were collected step wise over the range 2θ = 2-20 °, at steps of 0.02 °, an accumulation time of 20 s/step, using the Cu Kα radiation (λ = 1.54178 Å). UV-Vis optical spectroscopy of the perovskite films was carried out using a Cary 5G spectrophotometer and CaSO4 as reference. Field-emission scanning electron microscopy (FESEM) images were recorded with a Zeiss Ultra 55 field FESEM apparatus.
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