Prestige 21 fournier transformation infrared ftir spectrometer

The phase angle, crystal purity, and average crystallite size was determined using X-ray diffraction (XRD, PAN X’ Pert PRO, Cu-Kα λ = 1.5406 Å). The morphology and particle size were measured using the JEOL 648OLV scanning electron microscope and JEM 1230 transmission electron microscope (a SEM and TEM, respectively). For TEM studies, MgO nanopowder was ultrasonically dispersed in acetone for 30 min. A few droplets of this solution were collected on a carbon-coated Cu grid and dried in vacuum. Elemental analysis was performed using an energy dispersive X-ray (EDX) analyser, while a SHIMADZU Prestige 21 Fournier transformation infrared (FTIR) spectrometer was operated between 300–600 cm⁻¹ at room temperature to determine the molecular structure of the synthesized product.

The phase angle, crystal purity, and average crystallite size was determined using X-ray diffraction (XRD, PAN X’ Pert PRO, Cu-Kα λ = 1.5406 Å). The morphology and particle size were measured using the JEOL 648OLV scanning electron microscope and JEM 1230 transmission electron microscope (a SEM and TEM, respectively). For TEM studies, MgO nanopowder was ultrasonically dispersed in acetone for 30 min. A few droplets of this solution were collected on a carbon-coated Cu grid and dried in vacuum. Elemental analysis was performed using an energy dispersive X-ray (EDX) analyser, while a SHIMADZU Prestige 21 Fournier transformation infrared (FTIR) spectrometer was operated between 300–600 cm⁻¹ at room temperature to determine the molecular structure of the synthesized product.