Dodecanophenone

Manufactured by Merck Group

Sourced in United States

Dodecanophenone is a chemical compound that can be used as a laboratory reagent. It is a crystalline solid that is soluble in organic solvents. Dodecanophenone has a specific chemical structure and physical properties that make it useful for various research and analytical applications, but its precise function and intended use should not be extrapolated or interpreted without further information.

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4 protocols using dodecanophenone

Aqueous Solvent Preparation and Purity Validation

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Hydrochloric acid (1N Tritisol^TM), and sodium hydroxide (0.5N Tritisol^TM) were acquired from Merck (Darmstadt, Germany). Methanol (HPLC-grade) was obtained from Thermo Fisher Scientific (Waltham, MA, USA). Heptane (99%), dodecanophenone (98%), TTAB (>99%), 1-butanol (≥99.7%), 2-[Bis(2-hydroxyethyl)amino]-2-(hydroxymethyl)propane-1,3diol (Bis-tris) (>99%), and sodium phosphate dodecahydrate (>98%) were purchased from Sigma-Aldrich (St. Louis, MO, USA). Disodium hydrogen phosphate (99.5%) was from Baker (Phillipsburg, NJ, USA).
Test compounds with high purities were supplied from different manufacturers: Sigma-Aldrich, Merck, Baker, Carlo Erba (Milan, Italy), Fluka (St. Louis, MO, USA), Riedel-de Häen (Seelze, Germany), and Scharlab (Barcelona, Spain).

Fernández-Pumarega A., Martín-Sanz B., Amézqueta S., Fuguet E, & Rosés M. (2020). Estimation of the octanol-water distribution coefficient of basic compounds by a cationic microemulsion electrokinetic chromatography system. ADMET & DMPK, 8(1), 98-112.

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HPLC-MS Protocol for Chemical Analysis

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Methanol (HPLC-grade), hydrochloric acid (25 % in water), sodium hydroxide (>99%), sodium dihydrogenphosphate monohydrate (>99%), disodium hydrogenphosphate (>99%) and sodium dodecyl sulfate (>99%) were from Merck. Acetonitrile (HPLC grade) was from VWR International (West Chester, Pennsylvania, US). Taurocholic acid sodium salt monohydrate (98%) was from Acros Organics (Geel, Belgium) and Brij 35 was from Scharlab (Barcelona, Spain). Dodecanophenone (98%) was from Sigma-Aldrich. Water was purified by a Milli-Q plus system from Millipore (Bedford, MA, US), with a resistivity of 18.2 MΩ cm.
Tested substances were reagent grade or better and obtained from several manufacturers (Merck (Darmstadt, Germany), Sigma-Aldrich (St. Louis, MO, US), Carlo Erba (Milano, Italy), Baker (Center Valley, PA, US), Panreac (Castellar del Vallès, Spain), Thermo Fisher Scientific (Waltham, MA, US), Scharlab (Sentmenat, Spain).

Fernández-Pumarega A., Amézqueta S., Fuguet E, & Rosés M. (2015). Tadpole toxicity prediction using chromatographic systems. Journal of chromatography. A, 1418.

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Analytical Procedures for Diverse Compounds

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Sodium dihydrogen phosphate monohydrate (≥99%), dimethyl sulfoxide (DMSO, ≥99.9%), hydrochloric acid (1 N Titrisol TM ), and sodium hydroxide (0.5 N Titrisol TM )
were from Merck (Darmstadt, Germany). Methanol (HPLC grade) was obtained from Thermo Fisher Scientific (Waltham, MA, USA). Sodium dodecyl sulfate (SDS, ≥99%), 1-butanol (≥99.7%), heptane (99%), sodium phosphate dodecahydrate (>98%), and dodecanophenone (98%) were from Sigma-Aldrich (St. Louis, MO, USA). Disodium hydrogen phosphate (99.5%) and sodium acetate anhydrous (99.6%) were from Baker (Center Valley, PA, USA). Water was purified using a Milli-Q plus system from Millipore (Bedford, MA, USA), with a resistivity of 18.2 MΩ cm.
The test compounds were ibuprofen (≥98%), 2,4,6-trichlorophenol (98%), ketoprofen (≥98%), and naproxen (≥98%) from Sigma-Aldrich; benzoic acid (99.99%) from Baker; and 3-bromobenzoic acid (98%) from Merck.

Fernández-Pumarega A., Amézqueta S., Fuguet E, & Rosés M. (2019). Determination of the retention factor of ionizable compounds in microemulsion electrokinetic chromatography. Analytica chimica acta, 1078.

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Analytical Standards Characterization

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Sodium dihydrogen phosphate monohydrate (≥99%), dimethyl sulfoxide (≥99.9%), hydrochloric acid (Tritisol TM 1 N), ammonium chloride (>99.8%), and sodium hydroxide (Tritisol TM 0.5 N) were from Merck (Darmstadt, Germany). Methanol (HPLC grade) was from Thermo Fisher Scientific (Waltham, MA, USA). Sodium dodecyl sulfate (SDS, ≥99%), 1-butanol (≥99.7%), heptane (99%), sodium phosphate dodecahydrate (>98%), and dodecanophenone (98%) were from Sigma-Aldrich (St. Louis, MO, USA). Disodium hydrogen phosphate (99.5%) was from Baker (Phillipsburg, NJ, USA).
The solutes tested were of high purities and were acquired from Sigma-Aldrich, Baker, Merck, Carlo Erba (Milan, Italy), Fluka (St. Louis, MO, USA), Acros Organics (Geel, Belgium), and Riedel-de Haën (Seelze, Germany).
Water was purified using a Milli-Q plus system from Millipore (Burlington, MA, USA).

Fernández-Pumarega A., Amézqueta S., Fuguet E, & Rosés M. (2020). Estimation of the octanol-water distribution coefficient of acidic compounds by microemulsion electrokinetic chromatography. Journal of pharmaceutical and biomedical analysis, 179.

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