The chemicals such as zinc acetate, sodium hydroxide, titanium isopropoxide, isopropyl alcohol, were products of BDH, CDH (India), and Fisher (UK). All the solvents, including ethanol (99%), chloroform (99%), and methanol (99.99%), were from Blulax, India. Glacial acetic acid, potassium iodide, sodium bisulphate, hydrochloric acid (98%), ammonium chloride, ammonium hydroxide, Hanus solution, ferric chloride, sodium thioselphate, and potassium hydroxide were all from Sigma Aldrich UK. The chemicals and reagents used for this study were all of analytical grade. The functional group identification of WCO and BD were recorded using Infrared, Spectrum FTIR (PerkinElmer) spectroscopy. The crystal structure of the synthesized catalyst materials were investigated using X-ray diffraction (Drawell XRD-700, UK) at Jimma University, Jimma, south western Ethiopia.
Spectrum ftir
Manufactured by PerkinElmer
The Spectrum FTIR is a Fourier Transform Infrared Spectroscopy instrument manufactured by PerkinElmer. It is used to analyze the infrared spectra of samples, providing information about their molecular structure and composition.
Automatically generated - may contain errors
Lab products found in correlation
Sodium bisulphate, by Merck Group (1 mentions)
Ferric chloride, by Merck Group (1 mentions)
Ammonium hydroxide, by Merck Group (1 mentions)
Potassium hydroxide, by Merck Group (1 mentions)
Hydrochloric acid (hcl), by Merck Group (1 mentions)
Potassium iodide, by Merck Group (1 mentions)
Glacial acetic acid, by Merck Group (1 mentions)
Ammonium chloride, by Merck Group (1 mentions)
2 protocols using spectrum ftir
1
Synthesis and Characterization of Catalytic Materials
2
FTIR Analysis of Extruded Samples
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IR spectra of samples are
collected by Spectrum FTIR (Frontier, PerkinElmer). These are recorded
in transmission mode with attenuated total reflectance (ATR) assembly.
An extruded strip is placed on a ZnSe-based crystal surface in the
wave number range 4000–600 cm–1 with 16 scans
at a 4 cm–1 resolution for the analysis. A background
spectrum is collected prior to analysis to compensate the influence
of humidity and carbon dioxide present in air by subtracting spectra.
collected by Spectrum FTIR (Frontier, PerkinElmer). These are recorded
in transmission mode with attenuated total reflectance (ATR) assembly.
An extruded strip is placed on a ZnSe-based crystal surface in the
wave number range 4000–600 cm–1 with 16 scans
at a 4 cm–1 resolution for the analysis. A background
spectrum is collected prior to analysis to compensate the influence
of humidity and carbon dioxide present in air by subtracting spectra.
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