Powder XRD patterns of the nanoparticles were obtained from a Rigaku D/max Ultima III X-ray diffractometer with a radiation source of Cu-Kα (wavelength = 1.54174 Å) at 45 kV and 60 mA at a scanning step size of 0.020° in the 2θ range 10.015–80.012°. The XRD results were analyzed with the help of MATCH 3 software and the lattice parameters were calculated. The structural model was constructed on VESTA software. Scanning electron microscopic calculations were performed at 250 Quanta with a pressure of 70 (Pa) and 30 kV power. The patterns showed the cubic crystal structure of these nanoparticles. The catalytic reduction and absorption spectrum of the synthetic dye RB 5 was examined by a Halo DB 20 double beam spectrophotometer with the wavelength range of 400–700 nm. Investigation of the fuel properties by adding the newly synthesized graphene based tin cobalt oxide nanocomposite into the fuel to check the effect on the fuel efficiency was carried out in which the flash and fire point was monitored by the APEXJCX309 Closed Cup Flash Point Tester. An APEX-JCX406 oxygen bomb calorimeter was used to calculate the calorific value of the fuel. Specific gravity values were calculated by the gravity meter DA-640.
D max ultima 3 x ray diffractometer
Manufactured by Rigaku
The D/max Ultima III is an X-ray diffractometer manufactured by Rigaku. It is designed to analyze the crystalline structure of materials by measuring the diffraction of X-rays. The instrument provides accurate and reliable data for phase identification, quantitative analysis, and structural characterization of a wide range of materials.
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Lab products found in correlation
3 protocols using d max ultima 3 x ray diffractometer
1
Characterization of Graphene-based Tin Cobalt Oxide Nanocomposite
2
Comprehensive Characterization of Product
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Example 3
Characterization
The powder XRD patterns of the product were obtained from the prepared sample on a Rigaku D/max Ultima III X-ray diffractometer with a Cu-Ka radiation source (k=1.54174 Å) at 45 kV and 60 Ma at a scanning step size of 0.030° in the 2 h range 10.015°-79.982°. Scanning electron microscopic (SEM) observations were performed at Quanta 250 at a pressure of 70 Pa and 30 kV power. Catalytic reduction and absorption spectrum of anthraquinone dye drimarene red K-4BL was studied by a Halo DB 20 double beam spectrophotometer at a wavelength of 200-800 nm. Flash and fire point was supervised by APEXJCX309 Closed Cup Flash Point Tester. Specific gravity values were measured by Gravity meter DA-640 and calorific values were estimated by APEX-JCX406 Oxygen Bomb Calorimeter.
3
Comprehensive Materials Characterization Protocol
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X-ray powder diffraction (XRD) patterns were obtained on a Rigaku D/max Ultima III X-ray diffractometer with a Cu-Kα radiation source (λ = 0.15406 nm) operated at 40 kV and 150 mA at a scanning step of 0.02° in the 2θ range 10–80°. Scanning electron microscopy observation was performed on a JEOL JSM-6480A scanning electron microscope. Transmission electron microscopy (TEM) observation was performed on an FEI Tecnai G2 S-Twin TEM with an accelerating voltage of 200 kV. Thermo gravimetric was taken on NEZSCH STA 409 PC with a heating rate of 10 °C/min from 50 to 600 °C. UVD3500, Shimadzu was used to monitor the catalytic reduction of 4-NP.
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