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Ytterbium 3 acetate hydrate

Manufactured by Merck Group
Sourced in United States

Ytterbium(III) acetate hydrate is a chemical compound with the formula Yb(CH3COO)3 • xH2O. It is a white, crystalline solid that is soluble in water and other polar solvents. Ytterbium(III) acetate hydrate is commonly used as a source of ytterbium ions in various chemical and materials science applications.

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12 protocols using ytterbium 3 acetate hydrate

1

Synthesis of Lanthanide-Based Nanocrystals

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The materials including yttrium(III) acetate hydrate (99.9%), erbium(III) acetate hydrate (99.9%), ytterbium(III) acetate hydrate (99.99%), thulium(III) acetate hydrate (99.9%), holmium(III) acetate hydrate (99.9%), neodymium(III) acetate hydrate (99.9%), oleic acid (90%), 1-octadecene (90%), sodium hydroxide (NaOH; >98%), and ammonium fluoride (NH4F; >98%) were all purchased from Sigma-Aldrich. The nitrosonium tetrafluoroborate (NOBF4; 98%) was purchased from Alfa Aesar and indocyanine green (C43H47N2NaO6S2), N,N-dimethylformamide (DMF; anhydrous, 99.8%) were purchased from Energy Chemical. All these materials were used as received unless otherwise noted.
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2

Synthesis of Rare Earth Nanoparticles

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Dopamine hydrochloride was purchased from Alfa Aesar. Rare earth compounds of Yttrium (III) acetate hydrate ((CH3CO2)3Y·xH2O, 99.9%), YttErbium (III) acetate hydrate (Yb(C2H3O2)3·xH2O, 99.9%), Erbium (III) acetate hydrate ((CH3CO2)3Er·xH2O, 99.9%), Neodymium(III) acetate hydrate ((CH3CO2)3Nd · xH2O, 99.9%), 1-Octadecene (ODE, 90%), oleic acid (OA, 90%), ammonia fluoride (NH4F, ≥99.99% trace metals basis), IGEPAL® CO-520 ((C2H4O)n · C15H24O, ñ5), ammonium hydroxide solution (NH4OH, 28%) and 3-(4, 5-dimethylthiazol-2-yl)-2, 5-diphenyltetrazolium bromide (MTT) were purchased from Sigma/ Aldrich. Dulbecco’s modified Eagle’s medium (DMEM) and fetal bovine serum (FBS) were obtained from Thermo Fisher Scientific. All materials were used without further purification. Milli-Q water (18.2 MΩ cm) was used in all experiments.
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3

Synthesis of Lanthanide-based Nanoparticles

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Yttrium(iii) acetate hydrate (99.9%), ytterbium(iii) acetate hydrate (99.9%), erbium(iii) acetate hydrate (99.9%), and gadolinium(iii) acetate hydrate (99.9%) were purchased from Sigma-Aldrich. Sodium hydroxide (NaOH, >98%), ammonium fluoride (NH4F, >99.99%), 1-octadecene (ODE, 90%), and oleic acid (OA, 90%) were purchased from Aladdin®, China. Methanol (reagent grade), ethanol (reagent grade), and cyclohexane (reagent grade), and ferric nitrate (99.9%) were purchased from Sinopharm Chemical Reagent Co., China.
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4

Synthesis of Lanthanide Nanocrystals

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The lanthanide raw materials including erbium(III) acetate hydrate (99.9%), yttrium(III) acetate hydrate (99.9%), ytterbium(III) acetate hydrate (99.99%), holmium(III) acetate hydrate (99.9%), yttrium oxide (99.9%), ytterbium oxide (99.9%), yttrium(III) oxide (99.9%), ytterbium(III) oxide (99.9%) together with oleic acid (90%), 1-octadecene (90%), sodium hydroxide (NaOH; >98%), ammonium fluoride (NH4F; >98%), and trifluoroacetic acid (CF3COOH; >99%) were purchased from Sigma-Aldrich. The sodium trifluoroacetate (CF3COONa; >98%) were purchased from Alfa. All of these materials were used as received unless otherwise noted.
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5

Synthesis of Rare Earth Nanoparticles

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All chemicals were of analytical grade and were used without further purification. Rare earth acetates, Yttrium (III) acetate hydrate and Ytterbium (III)acetate hydrate with 99.9% trace metal basis were purchased from Sigma Aldrich. Erbium (III) acetate hydrate with 99.9% trace metal basis were purchased from Strem Chemicals. Oleic acid (90% technical grade), 1-Octadecene (90% technical grade), ammonium fluo-ride (≥ 99.99% trace metal basis), sodium hydroxide (semiconductor grade 99.99% trace metal basis), tetraethyl orthosilicate (≥ 99.0% G.C.), 3-mercaptopropyl trimethoxysilane (95%), 4-maleimidobutyric acid N-hydroxy-succinimide ester (≥ 98.0% HPLC), Polyvinylpyrrolidone were purchased from Sigma Aldrich. Ethanol was bought from Decon Laboratories Inc. while 10X Phosphate Buffered Saline was purchased from Lonza Inc. Ammonium hydroxide and Dimethyl sulfoxide (ACS Certified) and cyclohexane were purchased from Fisher Scientific.
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6

Synthesis of Rare Earth Acetate Nanoparticles

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The rare earth acetate hydrate salt precursors (RE(CH3COO)3.xH2O, 99.9%) including yttrium (III) acetate hydrate (Y(CH3COO)3.xH2O, 99.9%), ytterbium(III) acetate hydrate (Yb(CH3COO)3.xH2O, 99.9%), erbium(III) acetate hydrate (Er(CH3COO)3.xH2O, 99.9%) were purchased from Sigma-Aldrich. The oleic acid (OA, CH3(CH2)7CH = CH(CH2)7COOH, 99%), ammonium fluoride (NH4F, 98%), sodium acetate (CH3COONa, 99%), isopropanol (IPA, (CH3)2CHOH, 99%), cyclohexane (C6H12, 99%) and methanol (CH3OH, 99%) were purchased from Merck.
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7

Synthesis of Photosensitizer-Loaded Nanoparticles

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Erbium(III) acetate hydrate, lutetium(III) acetate hydrate, yttrium(III) acetate hydrate, yttErbium(III) acetate hydrate, neodymium(III) acetate hydrate, ammonium fluoride (NH4F), oleic acid (90%), 1-octadecene (90%), IGEPAL® CO-520, and ammonium hydroxide solution (28–30%) were purchased from Sigma–Aldrich (St. Louis, MO, USA). Tetraethyl orthosilicate (TEOS), 3-aminopropyltriethoxy-silane (APTES), and tetrakis(4-carboxyphenyl)porphyrin (TCPP) were purchased from Tokyo Chemical Industry (TCI) Co., Ltd. (Toshima, Kita-ku, Tokyo, Japan). mPEG2k-SC and FA/PEG5k-NHS were purchased from Biochempeg (Watertown, MA, USA). The HeLa (ATCC® CCL-2™) human adenocarcinoma cell line was obtained from the American Type Culture Collection (Rockville, MD, USA). DMEM and fetal bovine serum (FBS) were purchased from Capricorn (Ebsdorfergrund, Hesse, Germany). Trypsin-EDTA and penicillin-streptomycin (P/S) solution were purchased from Corning (Corning, NY, USA). The LIVE/DEADTM viability/cytotoxicity assay kit, LysoTrackerTM Green DND-26, and singlet oxygen sensor green reagent (SOSG) were purchased from Thermo Fisher Scientific (Waltham, MA, USA). All other reagents were obtained from Sigma–Aldrich unless otherwise indicated.
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8

Synthesis and Characterization of Multifunctional Nanoparticles

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The AIE PS of TBD was prepared as described in our previous work.47 (link) 1,2-Distearoyl-sn-glycero-3-phosphoethanolamine-N-[methoxy(polyethylene glycol)-2000]-Maleimide (DSPE-PEG-MAL) was purchased from Laysan. Cell Counting Kit-8 (CCK-8) was purchased from Dojindo. Calcein acetoxymethyl ester (calcein-AM) was purchased from Biolegend. 9,10-Anthracenediyl-bis(methylene)dimalonic acid (ABDA), tetrahydrofuran (THF), dimethyl sulfoxide (DMSO), propidium iodide (PI), yttrium(iii) acetate hydrate (99.9%), ytterbium(iii) acetate hydrate (99.9%), thulium(iii) acetate hydrate (99.9%) and neodymium(iii) acetate hydrate (99.9%) were purchased from Sigma-Aldrich. Sodium sulfate (98.0%), sodium hydroxide (NaOH, >98%), ammonium fluoride (NH4F, >99.99%), 1-octadecene (90%) and oleic acid (90%) were purchased from Aladdin®, China. Methanol (reagent grade), ethanol (reagent grade), and cyclohexane (reagent grade) were purchased from Sinopharm Chemical Reagent Co., China. Cyclic arginine-glycine-aspartic acid (cRGD) was synthesized by GL Biochem (Shanghai) Ltd. Chlorin e6 (Ce6, ≥98%) was purchased from Cayman Chemical Company. RPMI medium, DMEM medium, and phosphate buffered saline (PBS, 1×) were purchased from HyClone. Fetal calf serum was purchased from ScienCell. All the reagents were used without further purification.
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9

Synthesis and Characterization of Y1-x-y-zVO4:xHo3+/yYb3+/zK+ Phosphors

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The reagents used were
yttrium(III) acetate hydrate ((CH3CO2)3Y.xH2O, 99.99%), ytterbium(III) acetate
hydrate ((CH3CO2)3Yb.xH2O, 99.99%), holmium(III) acetate ((CH3CO2)3Ho.xH2O, 99.99%),
potassium carbonate (K2CO3, 99.99%), and ammonium
metavanadate (NH4VO3, 99.99%) and they were
purchased from Sigma-Aldrich. In addition, reagents like PEG (PEG
6000, 99.99%), EG (HOCH2CH2OH), sodium hydroxide
(NaOH), and dilute HCl acid were used as starting materials during
the synthesis of Y1–xyzVO4:xHo3+/yYb3+/zK+ (x = 1 at.%, y = 10 at.%, and z = 0, 2, 5, 7, and 10 at.%).
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10

Synthesis of Rare-Earth Oxide Nanoparticles

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Yttrium(III) acetate hydrate (99.9%), ytterbium(III) acetate hydrate (99.9%), thulium(III) acetate hydrate (99.9%), oleic acid (technical grade, 90%), 1-octadecene (technical grade, 90%), Igepal CO-520, tetraethyl orthosilicate (TEOS, >99.0%), ammonium fluoride (98%) sodium hydroxide (>98%), and Pluronic F127 were purchased from Sigma-Aldrich. Methanol (99.5%), cyclohexane (analytical grade), and ammonia solution (25–28%) were obtained from Aladdin. All chemicals were used as received without further purification.
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