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Formaldehyde dimethyl acetal

Manufactured by Merck Group
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Formaldehyde dimethyl acetal is a colorless, volatile liquid chemical compound. It is primarily used as a protective group in organic synthesis reactions, where it can temporarily mask the reactivity of a carbonyl group.

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Lab products found in correlation

1 2 dichloroethane, by Merck Group (2 mentions) Anhydrous ferric chloride, by Merck Group (2 mentions) Triptycene, by Merck Group (2 mentions) Chlorosulfonic acid clso3h, by Merck Group (1 mentions) Diphenylamine, by Merck Group (1 mentions) 1 naphthol, by Merck Group (1 mentions) Fecl3, by Merck Group (1 mentions) Ethanol, by Merck Group (1 mentions) Sodium hydroxide (naoh), by Merck Group (1 mentions) Methanol, by Merck Group (1 mentions) Sulfuric acid, by Merck Group (1 mentions) Tetrahydrofuran, by Merck Group (1 mentions) Isopropanol, by Merck Group (1 mentions) N n dimethylformamide (dmf), by Merck Group (1 mentions) Nitric acid, by Merck Group (1 mentions) Naphthalene, by Merck Group (1 mentions) Biphenyl, by Merck Group (1 mentions)

Close spelling variants of this product

Formaldehyde (1865 citations)

3 protocols using formaldehyde dimethyl acetal

1

Triptycene Synthesis and Characterization

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All purchased chemicals were at least reagent grade and were used without further purification. Triptycene (98.0%), anhydrous ferric chloride (FeCl3, ≥98.0%), 1,2-dichloroethane (DCE, 99.8%), and formaldehyde dimethyl acetal (FDA, ≥98.0%) were purchased from Sigma-Aldrich. Crown-ether-15 (98.0%) and all other solvents were purchased from TCI America. Deionized water was used to prepare all aqueous solutions.
Xu T., He Y., Qin Y., Zhao C., Peng C., Hu J, & Liu H. (2018). Facile preparation of porous organic copolymer based on triptycene and crown ether for efficient organic dye adsorption. RSC Advances, 8(9), 4963-4968.
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2

Synthesis and Characterization of Dye Compounds

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All of the purchased chemicals were of at least reagent grade and were used without further purification. Triptycene (98.0%), anhydrous ferric chloride (FeCl3, ≥98.0%), 1,2-dichloroethane (DCE, 99.8%), formaldehyde dimethyl acetal (FDA, ≥98.0%), and chlorosulfonic acid (ClSO3H, 99%) were purchased from Sigma-Aldrich. All of the other solvents were purchased from TCI America. The methylene blue (MEB, 99%), basic fuchsin (BF, 98%), and malachite green (MG, 98%), were purchased from Macklin Biochemical Co. Ltd. (Shanghai, China), and the above three dyes were used without further purification. Their structures are shown in Fig. 1.
Li C., He Y., Zhou L., Xu T., Hu J., Peng C, & Liu H. (2018). Fast adsorption of methylene blue, basic fuchsin, and malachite green by a novel sulfonic-grafted triptycene-based porous organic polymer. RSC Advances, 8(73), 41986-41993.
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3

Palladium-Catalyzed Bromination of Anisole

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4-Bromoanisole phenylboronic acid (PBA, 95%), biphenyl (BP, 99.5%), N,N-dimethylformamide (DMF, 99.8%), diphenylamine (DPA, 99%), formaldehyde dimethylacetal (dimethoxymethane, methylal, 99%), methanol (MeOH, 99.8%), naphthalene (NA, 99%), 1-naphthol (NL, ≥99%), nitric acid (HNO3, 70%), sulfuric acid (H2SO4, 96%), tetrahydrofuran (THF, ≥99.9%), ethanol (EtOH, ≥99.8%), isopropanol (i-PrOH, ≥99.5%), FeCl3 (anhydrous, ≥99.99%), and sodium hydroxide (NaOH, ≥98%) were purchased from Sigma-Aldrich, St. Louis, MO, USA. 1,2-Dichloroethan (1,2-DCE, 99.9%) was purchased from JSC “1 Base Chemical Reagents” (Staraya Kupavna, Russia). Palladium acetate (Pd(CH3COO)2, 47.68%ofPd) were obtained from JSC “Aurat”, Moscow, Russia. All chemicals were used as received. Distilled water was purified with an Elsi-Aqua water purification system.
Bakhvalova E.S., Bykov A.V., Markova M.E., Lugovoy Y.V., Sidorov A.I., Molchanov V.P., Sulman M.G., Kiwi-Minsker L, & Nikoshvili L.Z. (2023). Naphthalene-Based Polymers as Catalytic Supports for Suzuki Cross-Coupling. Molecules, 28(13), 4938.
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