Tris trimethylsilyl phosphine
Tris(trimethylsilyl)phosphine is a chemical compound used as a reagent in organic synthesis. It is a colorless, volatile liquid with the molecular formula P(SiMe3)3. The compound serves as a source of the phosphide anion and is commonly used in the preparation of other organophosphorus compounds.
Lab products found in correlation
6 protocols using tris trimethylsilyl phosphine
Synthesis of Colloidal Nanoparticles
Synthesis of Colloidal Nanocrystals
Synthesis of Colloidal Nanocrystals
99.99%), zinc(II) acetate (Zn(OAc)2, 99.99%), palmitic
acid (PA, C15H31COOH, 99.99%, stored at
−20 °C), gallium(III) chloride (beads, Sigma-Aldrich,
99.99%), tris(trimethylsilyl)-phosphine (P(TMS)3, 95%), 1-octadecene (ODE, 95%), oleic acid (Sigma-Aldrich,
99.99%), ammonium sulfide solution ((NH4)2S,
20% in H2O), 1-octadecene (ODE, 95%), formamide (FA, 99%),
dimethylformamide (DMF, 99%), Zn stearate (technical grade),
sulfur powder (99.98% trace metals basis), and trioctylphosphine
(TOP, 90% technical grade) were purchased from Sigma-Aldrich. Selenium
powder (99.98% trace metals basis) was purchased by Chem Pure. All
the chemicals were used without further purification.
Synthesis of Colloidal Semiconductor Nanocrystals
1-octadecene (ODE, technical grade, 90%), tris(trimethylsilyl)phosphine
(PTMS, 95%), trioctylphosphine (TOP, 97%), selenium (99.99%), palmitic
acid (HPA, >99%), indium acetate (In(Ac)3, 99.99% trace
metal basis), zinc acetate (Zn(Ac)2, 99.99% trace metal
basis), diethylzinc (≥52 wt % Zn basis), and di-n-butylmagnesium (1 M in heptane) were purchased from Sigma-Aldrich.
Ethanol (absolute, SupraSolv for GC-EDC/FID) was purchased from Merck.
Oleylamine (OLA, 80–90% C18, ≥96.0% (primary amine))
was purchased from Acros Organics. n-Hexane (anhydrous)
and sulfur (Puratronic , 99.9995%) were purchased from Alfa Aesar.
The used tris(trimethylsilyl)phosphine, diethylzinc, and di-n-butylmagnesium are spontaneously reactive with air
and moisture and should therefore be handled with care and solely
under inert atmosphere.
Synthesis of Quantum Dots
Synthesis of Indium-based Nanomaterials
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