For carbon, hydrogen, nitrogen and sulfur elemental content analysis, 8 mg of sample was introduced into a Thermo FlashEA 1112 Series analyzer.
Flashea 1112 series analyzer
Manufactured by Thermo Fisher Scientific
The FlashEA 1112 Series analyzer is an elemental analyzer designed for the determination of carbon, hydrogen, nitrogen, and sulfur in solid and liquid samples. It utilizes the dynamic flash combustion technique to perform elemental analysis with high precision and accuracy.
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Lab products found in correlation
2 protocols using flashea 1112 series analyzer
1
Elemental Content Analysis Protocol
2
Inert Conditions Reaction Characterization
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Reactions that
required inert conditions
were performed using modified Schlenk techniques or in an MBraun Unilab
glovebox under a nitrogen atmosphere. 1H and 13C NMR spectra were recorded on a Varian Unity Inova 400 MHz spectrometer. 1H and 13C NMR chemical shifts are given relative
to the residual proton or 13C solvent resonances. NMR spectra
were recorded at room temperature (20–25 °C) unless otherwise
noted. GC/MS data were collected on an Agilent 6890 Series GC connected
to a HP 5973 mass detector. Elemental analyses were performed using
a Thermo Electron Flash EA 1112 Series analyzer. Microwave heating
was conducted using a CEM Discover SP instrument in either 10 or 35
mL snap cap pressure tubes or in an open vessel mode. The temperature
of the reactions in the microwave was monitored using the floor-mounted
IR sensor in the instrument (external surface measurement).
required inert conditions
were performed using modified Schlenk techniques or in an MBraun Unilab
glovebox under a nitrogen atmosphere. 1H and 13C NMR spectra were recorded on a Varian Unity Inova 400 MHz spectrometer. 1H and 13C NMR chemical shifts are given relative
to the residual proton or 13C solvent resonances. NMR spectra
were recorded at room temperature (20–25 °C) unless otherwise
noted. GC/MS data were collected on an Agilent 6890 Series GC connected
to a HP 5973 mass detector. Elemental analyses were performed using
a Thermo Electron Flash EA 1112 Series analyzer. Microwave heating
was conducted using a CEM Discover SP instrument in either 10 or 35
mL snap cap pressure tubes or in an open vessel mode. The temperature
of the reactions in the microwave was monitored using the floor-mounted
IR sensor in the instrument (external surface measurement).
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