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N butyl methacrylate

Manufactured by Merck Group
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Sourced in United Kingdom, Denmark

N-butyl methacrylate is a clear, colorless liquid chemical compound. It is used as a raw material in the production of various polymer and copolymer products.

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Lab products found in correlation

4 4 azobis 4 cyanovaleric acid, by Merck Group (2 mentions) Trimethylsilyldiazomethane solution, by Merck Group (1 mentions) Benzyl bromide, by Merck Group (1 mentions) Ethyl methacrylate, by Merck Group (1 mentions) Deuterated acetone, by Merck Group (1 mentions) Dmaema, by Merck Group (1 mentions) 2 ethylhexyl methacrylate, by Thermo Fisher Scientific (1 mentions) N hexyl methacrylate, by Merck Group (1 mentions) 1 4 dioxane, by Merck Group (1 mentions) Triethanolamine, by Merck Group (1 mentions) Isopropanol, by Merck Group (1 mentions) Methyl methacrylate, by Merck Group (1 mentions) Diethyl ether, by Avantor (1 mentions) Cesium chloride, by Merck Group (1 mentions) Potassium thiocyanate, by Merck Group (1 mentions) Allyl methacrylate, by Merck Group (1 mentions) Acetonitrile, by Avantor (1 mentions) Lithium chloride (licl), by Merck Group (1 mentions) 2 2 2 trifluoroethanol, by Merck Group (1 mentions) Toluene, by Avantor (1 mentions)

2 protocols using n butyl methacrylate

1

Synthesis of Methacrylate Polymer Precursors

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Methyl
methacrylate (MMA, 99%), ethyl methacrylate
(EMA, 99%), n-butyl methacrylate (BMA, 99%), n-hexyl methacrylate (HMA, 99%), DMAEMA (99%), and MAA (99.5%)
were purchased from Sigma-Aldrich (Gillingham, U.K.) and were passed
through a basic alumina column to remove inhibitor prior to polymerization.
2-Ethylhexyl methacrylate (EHMA, 98%) was purchased from Alfa Aesar
(Heysham, U.K.), and its inhibitor was removed using an alumina column.
Isopropanol (IPA, 99.9%), triethanolamine (TEA, 99%), 4,4′-azobis(4-cyanovaleric
acid) (ACVA), 1,4-dioxane (99.5%), trimethylsilyldiazomethane solution
(2.0 M in diethyl ether), benzyl bromide (BzBr, 98%), and deuterated
acetone were purchased from Sigma-Aldrich. Deuterated chloroform (CDCl3) and deuterated dimethyl sulfoxide (DMSO-d6) for NMR spectroscopy measurements were purchased from
VWR (Lutterworth, U.K.). Deionized water was obtained using an Elgastat
Option 3A water purifier (Elga, High Wycombe, U.K.). 4-Cyano-4-(2-phenylethanesulfanylthiocarbonyl)sulfanylpentanoic
acid (PETTC) used for RAFT polymerization was prepared and purified
in-house, as reported previously.35 (link) Unless
stated otherwise, all materials were used as received.
Neal T.J., Parnell A.J., King S.M., Beattie D.L., Murray M.W., Williams N.S., Emmett S.N., Armes S.P., Spain S.G, & Mykhaylyk O.O. (2021). Control of Particle Size in the Self-Assembly of Amphiphilic Statistical Copolymers. Macromolecules, 54(3), 1425-1440.
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2

Synthesis of Functionalized Polymers

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Chemicals [2-(methacryloyloxy)ethyl]trimethylammonium chloride (METAC, 75 wt.% in H2O), 3sulfopropyl methacrylate potassium (SPMAK, 98%), 2-(dimethylamino)ethyl methacrylate (98%), 1,4-butane sultone (BS, ≥99%), 4-cyano-4-[(dodecylsulfanylthiocarbonyl)sulfanyl] pentanoic acid (CDPA, 97%), allyl methacrylate (AMA, 98%), n-butyl methacrylate (n-BMA, 99%), 3-mercaptopropyl trimethoxysilane (MPTMS, 95%), 2,2,2-trifluoroethanol (TFE, ≥99%), pentaerythritol tetrakis(3-mercaptopropionate) (PETMP, ≥95%), 4,4′-azobis(4-cyanovaleric acid) (ACVA, ≥98%), potassium chloride (KCl, 99.5%), potassium thiocyanate (KSCN, 99%), potassium bromide (KBr, 99%), lithium chloride (LiCl, 99%), and cesium chloride (CsCl, 98%) were purchased from Sigma-Aldrich Denmark. N,N-Dimethylformamide (≥99.9%), diethyl ether (≥99.9), toluene (≥99.8), and acetonitrile (≥99.9) were received from VWR Chemicals BDH and passed through activated basic aluminum oxide (Brockman I, Sigma-Aldrich) before use to remove any inhibitors. Zwitterionic monomer N-(2-methacryloylxyethyl)-N,N-diemthylammonium butanesulfonate (MABS) was prepared beforehand using the procedure reported in a previous study. 32 (link) Ultrapure water (Sartorius Arium Pro; 18.2 MΩ⋅cm) was used for preparing aqueous salt solutions.
Hegaard F., Biro R., Ehtiati K, & Thormann E. (2023). Ion-Specific Antipolyelectrolyte Effect on the Swelling Behavior of Polyzwitterionic Layers. Langmuir : the ACS journal of surfaces and colloids, 39(4).
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