by the three-electrode electrochemical workstation EC-Lab SP-150 potentiostat.
A platinum wire serves as the auxiliary electrode and the calomel
as the reference electrode. SEM tests were achieved by SEM Model Quanta
250 FEG (field emission gun) committed with an EDX unit, with accelerating
voltage of 30 kV, magnification 14 up to 1 000 000 (FEI
company, the Netherlands).