Sodium p-styrenesulfonate hydrate (TCI, > 93.0%) (NaStS); copper(I) bromide 98% (Sigma-Aldrich, Seoul, South Korea) (CuIBr); 4-(bromomethyl)benzoic acid 97% (Alfa Aesar, Seoul, South Korea) (BMB); 2,2′-bipyridine (bpy) 99.5% (Junsei, Tokyo, Japan); 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride (TCI, > 98.0%) (DMTMM); propiolic acid (TCI, > 97.0%) (PA); 1-hexylamine 99% (Sigma-Aldrich) (HA); and ninhydrin (TCI, > 98%) were used as received, without further purification. Silica gel 60 (Merck, 0.063-0.200 mm) was used for the column chromatography while tetrahydrofuran (Duksan, extra pure grade) (THF) was used to improve the purity of the polymer through solvent-precipitation. Deuterium oxide 99.9% D (Cambridge Isotope Laboratories, Inc., Seoul, South Korea) (D2O) was used as the NMR solvent. Polystyrene microparticles (5% w/v, 2.0–2.2 μm diameter) having surfaces functionalized with amine groups, were procured from Spherotech, IL, Illinois, USA.
1 hexylamine
Manufactured by Merck Group
Sourced in Japan, Australia, Belgium
1-hexylamine is a colorless, oily liquid organic compound with the chemical formula CH3(CH2)5NH2. It is a primary aliphatic amine and is commonly used as a chemical intermediate in the production of various compounds.
Automatically generated - may contain errors
Lab products found in correlation
Silica gel 60, by Merck Group (1 mentions)
Tetrahydrofuran, by Merck Group (1 mentions)
Ninhydrin, by Merck Group (1 mentions)
Copper 1 bromide, by Merck Group (1 mentions)
4 4 6 dimethoxy 1 3 5 triazin 2 yl 4 methylmorpholinium chloride, by Merck Group (1 mentions)
Sodium p styrenesulfonate hydrate, by Merck Group (1 mentions)
Propiolic acid, by Merck Group (1 mentions)
4 bromomethyl benzoic acid, by Thermo Fisher Scientific (1 mentions)
2 2 azobisisobutyronitrile aibn, by Merck Group (1 mentions)
Sodium citrate tribasic, by Merck Group (1 mentions)
Dopamine hydrochloride, by Merck Group (1 mentions)
Fluorobenzene, by Merck Group (1 mentions)
Nitric acid, by Merck Group (1 mentions)
Acetonitrile, by Avantor (1 mentions)
Oxalic acid, by Thermo Fisher Scientific (1 mentions)
Petroleum ether, by Avantor (1 mentions)
Glyoxal, by Thermo Fisher Scientific (1 mentions)
3 protocols using 1 hexylamine
1
Functionalized Polystyrene Microparticles
2
Synthesis and Characterization of Functionalized Polymers
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Dopamine hydrochloride (99%, DA), 2,3-dichloromaleic anhydride (97%), 1-hexylamine (99%), sodium citrate tribasic (≥99%), and fluorobenzene were purchased from Sigma-Aldrich (Sydney, Australia) and used as received without any further purification. Silver nitrate and triethylamine (TEA) were purchased from Univar (Sydney, Australia) and also used as received. 2,2′-azobis(isobutyronitrile) (AIBN, Sigma-Aldrich, 97%) was purified by recrystallization from cold methanol prior to use. Pentafluorostyrene (PFS, Oakwood Products, 99%) was passed through a column of activated basic alumina prior to use to remove inhibitor. 4-cyanopentanoic acid dithiobenzoate (CPADB) was synthesized as described in the literature [22 (link)]. 1-thio-β-ᴅ-glucose sodium salt (GluSNa) was prepared from 1-thio-β-ᴅ-glucose tetraacetate (AcO-GluSH) according to literature method [23 (link)]. All solvents were laboratory reagent grade and used as received without any further purification.
3
Synthesis of Alkylamine Derivatives
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Glyoxal (40 wt% in water), oxalic acid (98%, 144-62-7), and 1-octylamine (99+%, 111-86-4) were purchased from Acros Organics (Geel, Belgium). 1-Decylamine (98%, 2016-57-1) was purchased from TCI Europe (Zwijndrecht, Belgium). 1-Hexadecylamine (94%, 143-27-1) and 1-octadecylamine (≥85%, 124-30-1) were obtained from Merck (Heverlee, Belgium). 1-Hexylamine (99%, 111-26-2) and nitric acid (70 wt% in water, 7697-37-2) were bought from Sigma-Aldrich (Diegem, Belgium). 1-Dodecylamine (98%, 124-22-1) and 1-tetradecylamine (98%, 2016-42-4) were purchased from Janssen-Chemica (Beerse, Belgium). Acetic acid, glacial (100%, 64-19-7), hydrochloric acid (37 wt% in water, 7647-01-0) and formaldehyde (36 wt% in water, 50-00-0) were obtained from Fisher Scientific Limited (Loughborough, UK). Petroleum ether (bp 40–65 °C, technical grade) and acetonitrile (≥99.8%) were obtained from VWR (Heverlee, Belgium). Petroleum ether was distilled prior to use to remove high boiling residues. All other chemicals were used as received without further purification.
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