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Asap 2460 physisorption analyzer

Manufactured by Micromeritics
Sourced in United States

The ASAP 2460 physisorption analyzer is a laboratory instrument designed to measure the surface area and porosity of solid materials. It utilizes the principles of gas adsorption to determine the physical properties of sample materials. The ASAP 2460 provides accurate and reliable data on surface area, pore size distribution, and other related characteristics.

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2 protocols using asap 2460 physisorption analyzer

1

Characterization of Magnetic Adsorbent Material

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A vibrating sample magnetometer (VSM, 7410, LakeShore, Columbus, OH, USA) was used to measure the magnetic intensity of the AAM-MSMPM. Fourier transform infrared (FTIR) spectroscopy (Tensor II, Bruker, Billerica, Germany) was conducted in a scanning range of 4000 to 400 cm–1. The surface morphology of the adsorbents was measured at an accelerating voltage of 5.0 kV using scanning electron microscopy (SEM, SU-8220, Hitachi, Tokyo, Japan). The surface element composition and element valence of the AAM-MSMPM were measured in an Al Kα ray source and C 1s (284.6 eV) for calibration, using a photoelectron spectrometer (XPS, ESCALAB 250Xi, Thermo Fisher Scientific Inc., Carlsbad, CA, USA). The N2–BET surface areas and pore size distributions of the adsorbent were determined by N2 adsorption–desorption on an ASAP 2460 physisorption analyzer (Micromeritics, Norcross, GA, USA), and the specific surface area of the AAM-MSMPM was calculated by the Brunauer–Emmett–Teller (BET) equation. The Barrett–Joyner–Halenda (BJH) equation was used to calculate the pore volume and size distribution.
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2

Comprehensive Characterization of Hybrid Monolith

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The specific surface area of the hybrid monolith was calculated from nitrogen adsorption/desorption measurement using an ASAP 2460 physisorption analyzer (Micromeritics, U.S.A.). Hybrid monolith was first treated at 120 °C for 6 h in a vacuum before analysis. The specific surface area was calculated via the Brunauer–Emmett–Teller (BET) method, and the pore size distribution was determined from the adsorption isotherm by the Barrett–Joyner–Halenda (BJH) method. The total pore volume was determined at P/P0 = 0.99. Fourier transform infrared spectroscopy (FT-IR) characterization was carried out on Thermo Nicolet 380 spectrometer (Nicolet, Wisconsin, U.S.A.) using KBr pellets containing approximately 1 mg of sample and 100 mg of KBr. The microscopic morphology of hybrid monolithic materials was obtained by scanning electron microscopy (SEM, Hitachi, S-3000N). The macropores size distribution of the hybrid monolith was measured by the mercury intrusion porosimetry (MIP) method on PoreMasre GT-60 (Quantachrome Boynton Beach, U.S.A.). The analysis of S, P, and Ti contents in prepared Ti(IV)-IMAC hybrid monolith was carried out by inductively coupled plasma atomic emission spectrometry (ICP-AES) on a Vista-MPX (Varian, U.S.A.). Thermogravimetric (TG) data were collected in air atmosphere with heating at 10 °C/min on a Discover TGA (TA, U.S.A.).
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