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4 aminobenzonitrile

Manufactured by Merck Group
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Sourced in Germany, India

4-aminobenzonitrile is a chemical compound with the molecular formula C6H6N2. It is a crystalline solid used as a building block in the synthesis of various organic compounds.

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Lab products found in correlation

4 nitroaniline, by Merck Group (2 mentions) Aniline, by Thermo Fisher Scientific (1 mentions) 3 aminophenol, by Merck Group (1 mentions) 4 aminoaniline, by Merck Group (1 mentions) 2 meth oxy aniline, by Merck Group (1 mentions) 4 methoxyaniline, by Merck Group (1 mentions) 3 methoxyaniline, by Merck Group (1 mentions) 2 aminobenzonitrile, by Merck Group (1 mentions) 2 fluoroaniline, by Merck Group (1 mentions) 3 fluoroaniline, by Merck Group (1 mentions) 4 fluoroaniline, by Merck Group (1 mentions) 3 methylaniline, by Merck Group (1 mentions) 2 nitroaniline, by Merck Group (1 mentions) 3 nitroaniline, by Merck Group (1 mentions) Lc ms grade water, by Biosolve (1 mentions) Trifluoromethanesulfonic acid, by Merck Group (1 mentions) Phloroglucinol, by Merck Group (1 mentions) Hydrochloric acid (hcl), by Merck Group (1 mentions) Trifluoroacetic acid, by Merck Group (1 mentions) Anhydrous n n dimethylformamide, by Merck Group (1 mentions)

3 protocols using 4 aminobenzonitrile

1

Analytical Comparison of Mass Spectrometry Techniques

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For our investigation, we used the same compounds as for Paper-LTPI28 (link) and in a comparison between Paper-LTPI, ESI and APCI27 (link): 3-aminophenol, 2-fluoroaniline, 3-fluoroaniline, 4-fluoroaniline, 2-methoxyaniline (o-anisidine), 3-methoxyaniline (m-anisidine), 4-methoxyaniline (p-anisidine), 2-nitroaniline, 3-nitroaniline, 4-nitroaniline, 3-methylaniline (m-toluidine), 3-aminoaniline (m-phenylenediamine), 4-aminoaniline (p-phenylenediamine), 2-aminobenzonitrile, 3-aminobenzonitrile and 4-aminobenzonitrile from Sigma Aldrich (Taufkirchen, Germany); 2-methylaniline (o-toluidine), 4-methylaniline (p-toluidine) from Fluka (Buchs, Switzerland) and aniline from Acros (Geel, Belgium). Acetonitrile (ACN, LC–MS grade) was from VWR (Dresden, Germany) and water (LC–MS grade) from BIOSOLVE (Valkenswaard, Netherlands). 2-aminoaniline (o-phenylenediamine), 2-aminopyridine, 3-aminopyridine, 4-aminopyridine, 2-aminophenol, 4-aminophenol, 2-aminobenzoic acid, 3-aminobenzoic acid, 4-aminobenzoic acid, sulfanilic acid and 4-chloroaniline were kindly provided by Prof. em. S. Berger (University of Leipzig, Germany).
Kiontke A., Roudini M., Billig S., Fakhfouri A., Winkler A, & Birkemeyer C. (2021). Surface acoustic wave nebulization improves compound selectivity of low-temperature plasma ionization for mass spectrometry. Scientific Reports, 11, 2948.
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2

Synthesis of Triazine-Based Compounds

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Phloroglucinol was obtained from Sigma-Aldrich and used for the synthesis of 1,3,5-triformylPhloroglucinol (TFP).27 (link) 4-Aminobenzonitrile and trifluoromethanesulfonic acid were purchased from Sigma-Aldrich and used for the synthesis of 1,3,5-tris-(4-aminophenyl)-triazine (TAPT).19 (link) Anhydrous N,N-dimethylformamide, hexamine, trifluoroacetic acid and hydrochloric acid were obtained from Merck, India, and all were used without further purification.
Das S.K., Roy S., Das A., Chowdhury A., Chatterjee N, & Bhaumik A. (2022). A conjugated 2D covalent organic framework as a drug delivery vehicle towards triple negative breast cancer malignancy. Nanoscale Advances, 4(10), 2313-2320.
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3

Synthesis of Aryl Diazonium Salts

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Aryl diazonium salt D-NO 2 was prepared by the method published previously by our group. 35 2 g of 4-nitroaniline (≥99%, Sigma-Aldrich) and 10 mL of acetonitrile (≥99.9%, Sigma-Aldrich) were sequentially added to 12 mL of tetrafluoroboric acid (48% in H 2 O, Sigma-Aldrich). Then the mixed solution was transferred to an ice water bath and cooled down to 2 °C under continuous stirring. Afterwards, 2 mL of tert-butyl nitrite (90%, Sigma-Aldrich) was added to the reaction solution drop by drop. The solution was incubated for 30 min under stirring. After 3 times washes by diethyl ether (≥99.7%, Sigma-Aldrich), the resulting diazonium salt D-NO 2 was dissolved in acetone (≥99.9%, Sigma-Aldrich) and kept at room tempera-ture for drying. For the preparation of D-CCH and D-CN, 4-ethynylaniline (97%, Sigma-Aldrich) and 4-aminobenzonitrile (98%, Sigma-Aldrich) were used as corresponding precursors based on the same protocol.
Li D., Nizard P., Onidas D., Lamouri A., Pinson J., Mahouche-Chergui S., Aubertin K., Gazeau F., Luo Y, & Mangeney C. (2022). SERS tags derived from silver nanoparticles and aryl diazonium salts for cell Raman imaging. Nanoscale, 14(4).
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