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2 protocols using ammonium chloride nh4cl

1

Evaluation of Antioxidant and Digestive Enzyme Inhibition Activities

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ABTS (2,2′-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid)), Trolox (6-hydroxyl-2,5,7,8-tetramethylchroman-2-carboxylic acid), DPPH (2,2-diphenyl-1-picrylhydrazyl), TFA (trifluoroacetic acid), gallic acid, Folin–Ciocalteu reagent (FC), pepsin from porcine gastric mucosa-lyophilized powder, α-amylase and pancreatin from porcine pancreas, heat-stable α-amylase solution, protease, amyloglucosidase solution, 2-(N-Morpholino) ethanesulfonic acid (MES), and Tris (hydroxymethyl) aminomethane (TRIS) were purchased from Sigma-Aldrich Co. (St. Louis, MO, USA). Technical grades of methanol (MeOH) (>98.5%), ethanol (C2H5OH) (93%), sodium hydroxide (NaOH) (97%), sodium chloride (NaCl) (97%), potassium persulfate (K2S2O8) (100%), sodium carbonate (Na2CO3) (>99%), nitric acid (HNO3) (>99%), sulfuric acid (H2SO4) (>97%), hydrochloric acid (HCl) (37.2% w/w), petroleum ether (C6H14) (30–60 °C, A.R), Kjeldahl tablet (CuH10O9S), potassium chloride (KCl) (> 99%), sodium hydrogen carbonate (NaHCO3) (>99%), sodium chloride (NaCl) (97%), magnesium chloride (MgCl2) (99%), ammonium chloride (NH4Cl) (100%), calcium chloride (CaCl2) (>93%), monopotassium phosphate (KH2PO4), and indicators (tashiro and phenolphthalein) were purchased from VWR International (Leuven, Belgium). Inductively coupled plasma (ICP) multi-element standard solution IV was procured from Merck KGak (Darmstadt, Germany).
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2

Synthesis and Characterization of Silica-based Functional Materials

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The chemicals tetraethyl orthosilicate (TEOS), n-cetyltrimethylammonium bromide (CTAB), sodium hydroxide (NaOH), safranin O, budesonide, dichloromethane, 3-(triethoxysilyl)propyl isocyanate, acetonitrile, hydrochloric acid, 4-nitroaniline, sodium nitrite (NaNO2), N-phenyldiethanolamine, p-toluenesulfonyl chloride, pyridine, tetrahydrofuran (THF), methanol (MeOH) HPLC grade, sodium sulfide nonahydrate (Na2S·9H2O) were obtained from Aldrich. n-hexane and ethyl acetate were purchased from Scharlau. Sodium carbonate (Na2CO3), magnesium sulfate (MgSO4) and ammonium chloride (NH4Cl) were purchased from VWR.
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