Lead iodide (PbI2, 99.99%) was purchased from Tokyo Chemical Industry (TCI). Dimethylformamide (DMF) and lead bromide (PbBr2, >98%) were purchased from Alfa Aesar. FAI and FABr were purchased from GreatCell Solar. 2-Mercaptoethano (2-ME), dimethyl sulfoxide (DMSO), cesium iodide (CsI; 99.999%), and BCP (>96%) were purchased from Sigma-Aldrich. C60 (>99.55%) was purchased from Nano-C. Cr was purchased from K. J. Lesker. The nylon membranes were purchased from Sterlitech Corporation.
Lead iodide
Manufactured by Tokyo Chemical Industry
Sourced in Belgium
Lead iodide is an inorganic compound with the chemical formula PbI2. It is a yellow crystalline solid that is commonly used in various industrial and scientific applications.
Automatically generated - may contain errors
Lab products found in correlation
Chlorobenzene, by Merck Group (3 mentions)
Dimethyl sulfoxide (dmso), by Merck Group (3 mentions)
4 tert butylpyridine, by Merck Group (2 mentions)
2 propanol, by Merck Group (2 mentions)
Cesium iodide, by Merck Group (2 mentions)
Dimethylformamide, by Merck Group (2 mentions)
Dimethyl sulfoxide (dmso), by Samchun (2 mentions)
Cesium iodide, by Thermo Fisher Scientific (2 mentions)
4 tert butylpyridine tbp, by Merck Group (2 mentions)
Chlorobenzene, by Fujifilm (2 mentions)
Ethanolamine, by Samchun (2 mentions)
Dimethylformamide, by Samchun (2 mentions)
Lead bromide pbbr2, by Merck Group (2 mentions)
Zinc acetate dihydrate zn ch3co 2 2h2o, by Merck Group (2 mentions)
2 methoxyethanol, by Samchun (2 mentions)
Acetone, by Samchun (2 mentions)
Isopropanol, by Samchun (2 mentions)
Lead bromide, by Tokyo Chemical Industry (2 mentions)
Formamidinium iodide, by Greatcell Solar (2 mentions)
Methylammonium bromide, by Greatcell Solar (2 mentions)
8 protocols using lead iodide
1
Perovskite Solar Cell Fabrication
2
Perovskite Solar Cell Fabrication
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The 2.5 × 2.5 cm2 fluorine-doped
tin oxide glass slides (FTO OPV-FTO22-15,
sheet resistance of 14 Ω·sq–1) were purchased
from OPVTech. Titanium isopropoxide (Ti[OCH(CH3)2]4, 97%), hydrochloric acid (HCl, 37%), 2-propanol (for
HPLC, 99.9%), chlorobenzene (CB, anhydrous 99.8%), acetonitrile (ACN,
99.8%), 4-tert-butylpyridine (TBP, 98.0%), and cesium
iodide (CsI, 99.999%) were purchased from Sigma Aldrich. Lead iodide
(PbI2, 99.99%) was purchased from Tokyo Chemical Industry
(TCI). PbBr2 (99.999%), methyl ammonium bromide (MABr,
>99.5%), and formamidinium iodide (FAI, >99.5%) were purchased
from
Lumtec. Bis(trifluoromethane)sulfonimide lithium salt (Li-TFSI, 99.0%), N,N-dimethylformamide (DMF, anhydrous >99.5%),
2-bromoacetamide (98%), and 2-chloroacetamide (98%) were purchased
from Acros. Dimethly sulfoxide (DMSO, >99.7%), 2-iodoacetamide
(98%),
and dimethyl sulfoxide-d6 (DMSO-d6) were purchased from Merck. Spiro-OMeTAD was
purchased from Borun New Material Technology. All chemical substances
obtained commercially were used as purchased without further purification.
tin oxide glass slides (FTO OPV-FTO22-15,
sheet resistance of 14 Ω·sq–1) were purchased
from OPVTech. Titanium isopropoxide (Ti[OCH(CH3)2]4, 97%), hydrochloric acid (HCl, 37%), 2-propanol (for
HPLC, 99.9%), chlorobenzene (CB, anhydrous 99.8%), acetonitrile (ACN,
99.8%), 4-tert-butylpyridine (TBP, 98.0%), and cesium
iodide (CsI, 99.999%) were purchased from Sigma Aldrich. Lead iodide
(PbI2, 99.99%) was purchased from Tokyo Chemical Industry
(TCI). PbBr2 (99.999%), methyl ammonium bromide (MABr,
>99.5%), and formamidinium iodide (FAI, >99.5%) were purchased
from
Lumtec. Bis(trifluoromethane)sulfonimide lithium salt (Li-TFSI, 99.0%), N,N-dimethylformamide (DMF, anhydrous >99.5%),
2-bromoacetamide (98%), and 2-chloroacetamide (98%) were purchased
from Acros. Dimethly sulfoxide (DMSO, >99.7%), 2-iodoacetamide
(98%),
and dimethyl sulfoxide-d6 (DMSO-d6) were purchased from Merck. Spiro-OMeTAD was
purchased from Borun New Material Technology. All chemical substances
obtained commercially were used as purchased without further purification.
3
Perovskite Solar Cell Fabrication Protocol
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Lead iodide (PbI2, 99.99%, trace metal basis, TCI Chemicals) (553 mg) was dissolved in a mixture of dimethylformamide (Sigma-Aldrich, anhydrous, 99.8%) (0.876 mL) and dimethyl sulfoxide (Sigma-Aldrich, 99.9%) (0.0864 mL) and stirred overnight at 60 °C inside a nitrogen-filled glovebox. MAI (14.27 mg), 7.57 mg, and FAI (53.97 mg), obtained from Greatcell Solar Materials, were dissolved in 2-propanol (Sigma-Aldrich, 99.5%) (1 mL) and stirred overnight at 60 °C in a nitrogen-filled glovebox. PTAA (Mw = 14.5 kg mol−1, EM Index Co. Ltd) (3 mg) was dissolved in toluene (Sigma-Aldrich, anhydrous) (1 mL) and stirred overnight at 60 °C in a nitrogen-filled glovebox. PCBM (99%, Solenne BV) (20 mg) was dissolved in a 1:1 (v/v) mixture of chlorobenzene and chloroform (1 mL) and stirred overnight under ambient conditions. A dispersion of AZO nanoparticles (Avantama, 2.5 wt% in alcohols) was stirred overnight in a nitrogen-filled glovebox at ambient temperature.
4
Fabrication of Perovskite Solar Cells
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Indium-doped tin oxide (ITO)-coated glass slides (2 cm × 2 cm) with a sheet resistivity of 10 Ω/□ were obtained from AMG, Korea. The zinc acetate dihydrate (Zn(CH3CO)2∙2H2O, 99.99%), lead bromide (PbBr2, 99.99%), and 4-tert-butylpyridine (tBP) were purchased from Sigma Aldrich (St. Louis, MO, USA). Formamidinium bromide (FABr, 99.99%) was obtained from Greatcell Solar Materials Pvt Ltd. Lead iodide (PbI2, 99.99%) was acquired from TCI chemicals. Gold pellets (Au, 99.99%) and Poly(3-hexylthiophene-2,5-diyl) (P3HT) were bought from Rieke Metals Inc. (Lincoln, NE, USA). Cesium iodide (CsI, 99.99%) and tin oxide (SnO2, 15% in H2O) colloidal solutions were obtained from Alfa Aesar (Ward Hill, MA, USA). 2-methoxyethanol (2-ME, 99%), acetone (99%), ethanolamine (99%), dimethyl sulfoxide (DMSO, 99.8%), isopropanol (IPA, 99.5%), and dimethylformamide (DMF, 99.5%) were purchased from Samchun Chemical (Seoul, Republic of Korea). Phenyl-C61-butyric acid methyl ester (PC61BM, 99.5%) was bought from Organic Semiconductor Materials. Chlorobenzene (CB, 99% GR grade) was acquired from Wako Chemicals. All the received chemicals were used in the fabrication of PSCs without any further purification.
5
Perovskite and Organic Solar Cell Materials
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Lead iodide (PbI2, 99.99% trace metal basis) and lead bromide (PbBr2, >98%) were purchased from TCI Chemicals. Methylammonium bromide (MABr) and formamidinium iodide (FAI) were purchased from Greatcell Solar Materials. Potassium iodide (KI, 99.999%) and cesium iodide (CsI, 99.999%) were purchased from Fisher Scientific and Sigma-Aldrich, respectively. [2-(9H-carbazol-9-yl)ethyl] phosphonic acid (2PACz, >98.0%) was purchased from TCI Chemicals. [6,6]-phenyl-C61-butyric acid methyl ester (PCBM, 99%) was purchased from Solenne BV. PM6 was purchased from Solarmer Materials. Tin(IV) oxide (SnO2 nanoparticles, 15 wt% in water) was purchased from Alfa Aesar. Dimethylformamide (DMF, 99.8%), dimethyl sulfoxide (DMSO, anhydrous 99.9%), anisole (99.7%), propan-2-ol (IPA, 99.95%), and chlorobenzene (CB, 99.8%) were purchased from Sigma-Aldrich. Ethanol (>95%) was purchased from Acros Organics.
6
Perovskite Solar Cell Fabrication
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All organic solvents—dimethylformamide (DMF), dimethyl sulfoxide (DMSO), chlorobenzene (CB), isopropyl alcohol (IPA), and acetonitrile (ACN)—were purchased in anhydrous, ultra-pure grade from Sigma Aldrich (Munich, Germany), and used as received. Solar cells were fabricated on SnO2:F (FTO) coated glass TEC8 from GreatCellSolar (Queanbeyan, Australia). The precursor for NiO hole transporting layer—Tris (ethylenediamine) nickel acetate (TED-NiA)—was synthesized accordingly to the route described in previous work and dissolved in 1.0 M concentration in ethylene glycol (analytical grade). Copper iodide (99.999% trace metal basis, powder) was purchased from Sigma Aldrich. Lead Iodide (99.99%, trace metals basis from TCI Chemicals, Zwijndrecht, Belgium) and methylammonium iodide (MAI, 99.99% purity from GreatcellSolar) were used for perovskite ink. Phenyl-C61-butyric acid methyl ester (PCBM, >99% purity) and bathocuproine (BCP, >99.8% sublimed grade) were purchased from Osilla Inc. (Sheffield, UK) and used for electron transport layers (ETLs) fabrication.
7
Fabrication of Perovskite Solar Cells
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Indium-doped tin oxide (ITO)-coated glass slides (2 cm × 2 cm) with a sheet resistivity of 10 Ω/□ were obtained from AMG, Korea. The zinc acetate dihydrate (Zn(CH3CO)2∙2H2O, 99.99%), lead bromide (PbBr2, 99.99%), and 4-tert-butylpyridine (tBP) were purchased from Sigma Aldrich (St. Louis, MO, USA). Formamidinium bromide (FABr, 99.99%) was obtained from Greatcell Solar Materials Pvt Ltd. Lead iodide (PbI2, 99.99%) was acquired from TCI chemicals. Gold pellets (Au, 99.99%) and Poly(3-hexylthiophene-2,5-diyl) (P3HT) were bought from Rieke Metals Inc. (Lincoln, NE, USA). Cesium iodide (CsI, 99.99%) and tin oxide (SnO2, 15% in H2O) colloidal solutions were obtained from Alfa Aesar (Ward Hill, MA, USA). 2-methoxyethanol (2-ME, 99%), acetone (99%), ethanolamine (99%), dimethyl sulfoxide (DMSO, 99.8%), isopropanol (IPA, 99.5%), and dimethylformamide (DMF, 99.5%) were purchased from Samchun Chemical (Seoul, Republic of Korea). Phenyl-C61-butyric acid methyl ester (PC61BM, 99.5%) was bought from Organic Semiconductor Materials. Chlorobenzene (CB, 99% GR grade) was acquired from Wako Chemicals. All the received chemicals were used in the fabrication of PSCs without any further purification.
8
Perovskite Solar Cell Fabrication
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Cesium iodide (CsI 99.9%), lithium bis(trifluoromethanesulfonyl)imide (Li‐TFSi 99.95%), 4‐tert‐butylpyridine (TBP, 98%), N,N‐dimethylformamide (DMF, 99.8%), dimethyl sulfoxide (DMSO, 99.9%), chlorobenzene (99.8%) were purchased from Sigma‐Aldrich. Formamidinium iodide (FAI, 99.9%), Formamidinium iodide (FABr, 99.9%), methylammonium bromide (MABr, 99.9%) were purchased from Greatcell Solar. Lead iodide (PbI2, 99.99%) and lead bromide (PbBr2, 99.99%) were purchased from TCI chemicals. SnO2 nanoparticle solution (15 wt% in DI water) was purchased from Alfa Aesar. VNPB and Spiro‐OMeTAD were purchased from Lumtec. PEDOT:PSS (AI 4083) was purchased from Clevios Corporation. PC60BM was purchased from 1‐Materials.
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