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5 protocols using p xylene

1

Volatile Organic Compound Extraction

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Benzene, 99.5%, ethylbenzene, 99%, o-xylene, 99%, p-xylene, 99%, and trichloromethane, 99.8% were purchased form Alfa Aesar (Ward Hill, MA). Acetone, 99.9%, and dichlormethane, 99.5%, were purchased form Pharmco AAPER (Brookfield, CT). Toluene, 99.9%, was purchased from Fisher Scientific (Pittsburgh, PA). SPME fibres and Thermogreen® LB-2 Septa were obtained from Supelco (St. Louis, MO). Helium gas used as carrier gas in GC-MS was supplied by Airgas (Radnor, PA).
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2

Analytical Determination of Aromatic Hydrocarbons

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All chemicals used were analytical grade purity: benzene (99%, Beantown Chemical, New Hampshire), toluene (99.8%, Sigma Aldrich, Missouri), ethylbenzene (99.8%, Acros Organics, Massachusetts), o-xylene, m-xylene, p-xylene (99%, Alfa Aesar, Massachusetts), MTBE, TBA (99%, TCI America, Oregon), isobutane (99.99%, Gas Innovations, Texas), 1-butanol (99.4%, Acros Organics, Massachusetts), 2-butanol (99%, Sigma Aldrich, Missouri).
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3

Synthesis of Fluorescent Nanoparticles

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Manganese (II) acetate, oleylamine, oleic acid, iron (II) perchlorate, and 2-(N-morpholino) ethanesulfonic acid (MES) were purchased from Sigma-Aldritch. p-Xylene, dimethyl sulfoxide (DMSO), dihydrocaffeic acid (DHCA), and fluorescein isothiocyanate (FITC) were purchased from Acros Organics. 1-ethyl-3-[3-dimethylaminopropyl]carbodiimide (EDC) and N-hydroxysuccinimide (NHS) were purchased from Thermo Scientific. Dextran, amino, 40000 MW was purchased from Molecular Probes. dihydrocaffeic acid was purchased from Alfa Aesar.
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4

Synthesis of Polymer Composites

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All chemicals were used as purchased without further purification. RuCl3.3H2O, RhCl3.3H2O, PdCl2, IrCl3.3H2O and K2PtCl4 were purchased from PreciousMetalsOnline. CeO2, hexylamine, hexanoyl chloride and 5% Ru/C were purchased from Sigma-Aldrich. 5% Pt/C was purchased from Alfa Aesar. p-Xylene was purchased from Acros Organics. PE (powder), PA-6 (resins, Mn = 27,380 g/mol), PA-66 (resins, Mn = 47,240 g/mol), PA-12 (resins, Mn = 27,060 g/mol), PA-612 (resins, Mn = 14,730 g/mol), 30% carbon-fibre PA-66 composite (resins, Mn = 19,920 g/mol) and 30% glass-fibre reinforced PA-6 rods were purchased from Sigma-Aldrich. The rods were sawn into smaller pieces before reaction. Ultramid® C40 L (resins, Mn = 49,010 g/mol) was provided by BASF. Gel permeation chromatography was used to measure the Mn of all resins, except for PE and the PA composites. PA-66 fishing net was purchased from Stucki Thun.
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5

Synthesis of Copper Nanoparticles

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Copper (II) chloride dehydrate (CuCl2·2H2O) was purchased from J.T.Baker, Phillipsburgc, NJ, USA. Glucose (Dextrose monohydrate, C6H12O6·H2O) and hexadecyl amine (HDA, C16H35N) were obtained from Sigma-Aldrich, St. Louis, MO, USA. The p-Xylene (99%) was purchased from Acros, St. Louis, MO, USA, and PEG-7 Glyceryl Cocoate was provided from KOLB, Hedingen, Switzerland, while the ethanol (C2H5OH, 95%) was from Echo Chemical Co., Miaoli, Taiwan. All chemicals were used as received without further purification. The pellet form of isotactic polypropylene, i-PP (PC6501), was provided by Lee Chang Yung Chemical Industry Co., Taipei, Taiwan. The Mv and density were 280,000 g/mole and 0.90 g/cm3, respectively.
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