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2 protocols using chloroacetic acid

1

Graphite-based Composite Synthesis

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Graphite
powder was provided
from Alpha Chemika. Zirconium oxychloride, 1,4-benzene dicarboxylic
acid, copper sulfate, and methylene blue were purchased from MP Biomedicals,
LLC. Sodium alginate was used as received (M/G ratio of the alginate
= 1.5, Mw = 6.4 × 104 g/mol, viscosity:
200 ± 20 mPa·s 1% wt (25 °C), Shanghai McLean Biochemical
Technology Co., Ltd., China). Hydrogen peroxide, chloroacetic acid, N,N-dimethyl formamide, and hydrochloric
acid were bought from Loba Chemie. Potassium permanganate, methanol,
and ethanol were supplied by Aladdin Reagent Co., Ltd. Sodium hydroxide,
calcium chloride, sodium nitrate, and sulfuric acid were obtained
from Sinopharm Chemical Reagents.
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2

Graphite-Based Nano-Adsorbent Synthesis

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Graphite powder was derived from Alfa-Aesar Co. (UK). Potassium permanganate (≥99%), sodium nitrate (≥99%), zirconium oxychloride (99.5%), sulphuric acid (97%) and hydrochloric acid (37%) were supplied by Rankem (India). Hydrogen peroxide (35%), N,N-dimethyl formamide (99%), ethanol (99%) and methanol (99.9%) were bought from Merck. Chloroacetic acid (99.5%) and sodium hydroxide (97%) were obtained from Loba Chemie Ltd (India). Ferric chloride hexahydrate (99%), 1,4-benzene dicarboxylic acid (98%) and methylene blue dye were supplied by Merck.
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