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Oxford gemini

Manufactured by Agilent Technologies
Sourced in United States

The Oxford Gemini is a compact and versatile lab equipment designed for a range of analytical applications. It features high-performance capabilities and precise measurements. The core function of the Oxford Gemini is to provide reliable and accurate data for researchers and scientists.

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2 protocols using oxford gemini

1

Comprehensive Characterization of Carbon Nanodots

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Atomic force microscope (AFM, Agilent Technologies 5600 LS Series) and transmission electron microscopy (TEM, Carl Zeiss Libra 120 Plus) were used to study the size of the CNDs. Fourier transform infrared spectroscopy (FTIR, Varian 670), Raman spectroscopy (Horiba XploRA One Raman Confocal Microscope System), X-ray photoelectron spectroscopy (XPS, Thermo Fisher ESCALAB 250 Xi), and X-ray powder diffraction (XRD, Agilent Technologies Oxford Gemini) were used to determine the elemental composition and chemical structure of the CNDs. A Zetasizer nano-ZX (Malvern Instruments ZEN3600) was used to study the stability of the CNDs as a function of pH (Fisher Scientific pH 2100). Ultraviolet-visible spectroscopy (UV-Vis spectroscopy, Varian Cary 6000i) and fluorescence spectroscopy (Varian Cary Eclipse) were used to investigate the absorbance and fluorescence properties of the CNDs, respectively.
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2

Synthesis and Characterization of Carbon Nanodots

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Carbon nanodots (CNDs) were synthesized and characterized following our published method [44 (link),45 (link)]. Briefly, CNDs were synthesized by mixing 0.96 g of citric acid (CA) and 1 mL of Ethylenediamine (EDA) in 1 mL of deionized water. The solution was heated in a microwave synthesizer (CEM Corp 908005 (Matthews, NC, USA)) at 300 W for 10 min. To purify the CNDs, the solid was dissolved in DI water and dialyzed through a dialysis membrane with MWCO (molecular weight cut out) of 1000 Da for 24 h. The structure of CNDs was characterized using Fourier transform infrared spectroscopy (FTIR, Varian 670 (Palo Alto, CA, USA), and the size and morphology were characterized by atomic force microscopy (AFM, Agilent 5600LS (Santa Clara, CA, USA)). X-ray diffraction (XRD, Agilent Technologies Oxford Gemini, The Woodlands, TX, USA) was used to analyze the crystal structure of the CNDs. To study the chemical content and the structure of the CNDs, Fourier transform infrared spectroscopy (FTIR) was performed. The fluorescence intensity peaks were measured using a Cary fluorescence spectrophotometer to find the emission and excitation wavelengths for the CNDs. The CND concentration in distilled water for analysis was 0.06 mg/mL. The surface chemistry of CNDs was studied using carbon 1s X-ray photoelectron spectroscopy (XPS, ESCALAB 250 Xi, Thermo Fisher, West Sussex, UK).
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