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2 protocols using linalool

1

Comprehensive Volatile Compound Analysis Protocol

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Methanol (HPLC grade) was purchased from Merck (Darmstadt, Germany) NaCl (analytical grade) was purchased from Sinopharm Chemical Reagent Co., Ltd (Beijing, China); and pure water was obtained from the Milli-Q purification system (Millipore, Bedford, MA).
The chemical standards were purchased as follows: (Z)-3-hexenal, 2-octanol, hexanal, (E)-2-hexenal, geranic acid, phellandrene, β-myrcene, β-damascenone, D-limonene, citronellol, benzyl alcohol, neral, α-terpineol, geranial, geraniol, rose oxide II (cis), rose oxide I (trans), phenylethyl alcohol from Sigma (St. Louis, MO, USA); octanoic acid, pentanal, octanal, nonanal, benzaldehyde, 3-methylbutanal, hexanoic acid, (Z)-3-hexenol, 1-octen-3-ol, heptanol, ethyl acetate, ethyl butyrate, ethyl isobutyrate, butyl acetate, ethyl pentanoate, methyl salicylate, hexyl acetate, (E)-2-hexenoic acid, P-cymene, terpinolene, linalool, 4-terpineol, geranyl acetone from Dr. Ehrenstorfer (Germany); β-ionone from Fluka (Buchs, Switzerland); ethyl hexanoate from Nu-chek (USA); octanol, hexanol, (E)-2-hexenol from Chem Service (USA), and n-alkanes (C7-C27) from Supelco (Bellefonte, PA).
The automatic solid-phase microextraction (SPME) fibres of 50/30 μm divinylbenzene/carboxen/polydimethylsiloxane (DVB/CAR/PDMS) were purchased from Supelco (Bellefonte, PA, USA).
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2

Precise Analytical Procedures for Plant Extracts

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High purity reagents were used: Ethanol absolute, puriss p.a., Acetic acid puriss (99,8-100,5%) and Ammonium hydroxide solution puriss p.a. (~ 25% NH3 basis) were purchased from Honeywell, Sodium hydroxide pellets from Bernd Kraft, Sodium trisilicate (≥ 18% Na basis and ≥ 60% Si basis) from Sigma-Aldrich, Linalool from Dr. Ehrenstorfer; p-Cymene from Chromadex; isomers α+β Thujone, Myrcene, and Eucalyptol from Sigma-Aldrich, each of them with the certified value of purity, Ethyl acetate from Carlo Erba, Stearic acid from Sigma-Aldrich. During the entire study, water was obtained from the Milli-Q equipment.
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