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2 protocols using 1 3 5 triformylphloroglucinol

1

Synthesis and Characterization of Fluorescent Silica Nanoparticles

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The standards of ferulic acid, cinnamic acid, syringic acid, and caffeic acid were purchased from Acros Organics (Morris Plains, NJ, USA). 1,3,5-triformylphloroglucinol (TP; 99%) was purchased from Strem Chemicals, Inc., Newburypor, MA, USA. P-phenylenediamine (Pa) and mesitylene (99%) were purchased from Shanghai Macklin Biochemical Co., Ltd., Shanghai, China. CdSe/ZnS quantum dots with fluorescence excitation wavelength at 460 nm and emission centered at 605 nm were purchased from Jiayuan (Wuhan, China). Triton X-100 (99.5%), cyclohexane (99.5%), 3-aminopropyl triethoxysilane (APTES; 98%), and acetic acid (99.5%) were purchased from Sinopharm Chemical Reagent Co., Ltd., Beijing, China. Tetraethyl orthosilicate (TEOS; 98%) were purchased from J&K Scientific Ltd., Beijing, China. All reagents were at least analytical grade and purchased from Beijing Chemicals (Beijing, China). Doubly deionized water (DDW, 18.2 MΩ cm−1) was obtained from a Water Pro water purification system (Labconco, Kansas City, MO, USA).
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2

Synthesis and Characterization of Fluorescent Nanoparticles

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QCA (95%) was purchased from Adamas Reagent Co., Ltd., Shanghai, China. Olaquindox (QLA; 99%), and carbadox (CBX; 98.5%) was purchased from Dr. Ehrenstorfer GmbH Co., Ltd., Augsburg, Germany. Mequindox (MEQ; 99.6%) was purchased from the Institute of Veterinary Drug Control, Beijing, China; 3-Methylquinoline-2-carboxylic acid (MQCA; 95%) was purchased from Aladdin Bio-Chem Technology Co., Ltd., Shanghai, China. CdSe/ZnS QDs with 460 nm excitation and 605 nm fluorescence emission were purchased from Jiayuan (Wuhan, China); 1,3,5-triformylphloroglucinol (TP; 99%) was purchased from Strem Chemicals, Inc., Newburyport, MA, USA. P-phenylenediamine (Pa) and mesitylene (99%) were purchased from Shanghai Macklin Biochemical Co., Ltd., Shanghai, China; 3-Aminopropyl triethoxysilane (APTES; 98%), acetic acid (99.5%), Triton X-100 (99.5%), and cyclohexane (99.5%) were purchased from Sinopharm Chemical Reagent Co., Ltd., Beijing, China. Dioxane (99.5%) and tetraethyl orthosilicate (TEOS; 98%) were purchased from J&K Scientific Ltd., Beijing, China. Doubly de-ionized water (DDW; 18.2 MΩ cm−1) was obtained from a Water Pro water purification system (Labconco, Kansas City, MO, USA).
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