Avb 400 mhz nmr spectrometer

¹H NMR spectra were collected on a Bruker AV-300 MHz NMR spectrometer, a Bruker AVB-400 MHz NMR spectrometer, or a Bruker AVQ-400 MHz NMR spectrometer, as indicated in the figure captions in the Supporting Information. Laboratory powder X-ray diffraction patterns were collected using a Bruker AXS D8 Advance diffractometer with Cu Kα radiation (λ = 1.5418 Å). All synthetic manipulations were carried out under air unless noted otherwise. All solvents and diamines were purchased from commercial sources and used without additional purification. All chiral additives were purchased from commercial vendors and used without purification. The ligand H₄dobpdc was purchased from Hangzhou Trylead Chemical Technology Co.