PM6, Y6, BTP-eC9, IEICO-4F, and ITCC were purchased from 1-Materials (Quebec, Canada). PBDTTT-OFT was received from Toray Industries. PC71BM was purchased from Solenne BV Corporation. The precursor (ECRIOS VICT-Cz) of transparent polyimide was from Mitsui Chemicals (Japan). Zinc acetate dehydrates, 2-methoxyethanol, chloroform, and chlorobenzene were purchased from FUJIFILM Wako Pure Chemical Corporation (Japan). Ethoxylated polyethyleneimine (PEIE, 80% ethoxylated solution, 37 wt% in H2O), 1-chloronaphthalene (1-CN), and 1,8-diiodooctane (DIO) were purchased from Sigma-Aldrich. All materials were used as received without further purification.
1 8 diiodooctane dio
Manufactured by Merck Group
1,8-Diiodooctane (DIO) is a chemical compound used as a laboratory reagent. It is a colorless, viscous liquid with a high boiling point. DIO is commonly utilized in various scientific applications, such as organic synthesis, materials science, and biochemical research. The primary function of DIO is to serve as a solvent, a coupling agent, or a synthetic intermediate, facilitating specific chemical reactions and processes. Detailed information about the intended use or applications of DIO is not provided to maintain an unbiased and factual approach.
Automatically generated - may contain errors
Lab products found in correlation
Chloroform, by Fujifilm (1 mentions)
Chlorobenzene, by Fujifilm (1 mentions)
Pbdttt oft, by Toray (1 mentions)
2 methoxyethanol, by Fujifilm (1 mentions)
Chlorobenzene cb, by Merck Group (1 mentions)
It 4f, by Solarmer (1 mentions)
Pm6 pbdb t 2f, by Solarmer (1 mentions)
1 chloronaphthalene cn, by Merck Group (1 mentions)
Chloroform, by Merck Group (1 mentions)
Chlorobenzene, by Thermo Fisher Scientific (1 mentions)
Ethanolamine nh2ch2ch2oh, by Merck Group (1 mentions)
2 methoxyethanol ch3och2ch2oh, by Merck Group (1 mentions)
5 protocols using 1 8 diiodooctane dio
1
Organic Photovoltaic Material Procurement
2
Organic Solar Cell Material Preparation
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All chemicals and solvents for the imine synthesis were of reagent grade and were obtained from Aldrich Chemical Co (Saint Louis, MO, USA). The most important ingredients for solar cell construction: poly[[4,8-bis[(2-ethylhexyl)oxy]benzo[1,2-b:4,5-b′]dithiophene-2,6-diyl][3-fluoro-2-[(2-ethylhexyl)carbonyl]thieno[3,4-b]thiophenediyl]] (PTB7) (M215 butch), [6,6]-phenyl-C70-butyric acid methyl ester (PC70BM), poly(3,4-ethylenedioxythiophene) polystyrene sulfonate (PEDOT:PSS) (Heraeus Clevios AI 4083), and indium tin oxide (ITO) 8 pixel glass substrates were purchased from Ossila. Solvents for active layer preparation: chlorobenzene (CB) and 1,8-diiodooctane (DIO) were purchased from Sigma-Aldrich.
3
Organic Photovoltaic Fabrication and Characterization
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PM6 (PBDB‐T‐2F) and IT‐4F, ITIC, Y6, and N3 were purchased from Solarmer Materials Inc., Beijing. L8‐BO was purchased from Guangzhou Chasing Light Technology Co., Ltd. 2‐phenylethylmercaptan (PET), Zn(OAc)2, TMAH, and chlorobenzene (CB, 99.8%) were purchased from J&K Scientific Ltd. 1,8‐diiodooctane (DIO) and 1‐chloronaphthalene (CN) was purchased from sigma‐Aldrich. Molybdenum (VI) oxide (MoO3) was purchased from Sterm Chemicals. All materials were used as received without further purification. ZnO was prepared through the reaction of TMAH and Zn(OAc)2 in DMSO as reported by Qian et al.[33 ]
4
Synthesis of Organic Semiconductors
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PBT1‐C, PBT1‐C‐2Cl, TTPTTT‐4F, O‐INIC3, and PT2 were synthesized in the lab according to the literature.[10 , 24 , 27 , 28 , 44 , 45 ] It should be noted that both O‐INIC3 and EH‐INIC3 shared the same central core with originally reported INIC3,[44 ] but differed in side chains. And the coplymers PT1 and PT3 were synthesized by changing the T1‐2Cl/T1 ratios according to the literature.[45 ] Y6 was purchased from HYPER Inc. (Zhejiang, China). Zinc acetate dihydrate (Zn(CH3COO)2·2H2O) was purchased from Alfa Aesar. Chlorobenzene, chloroform, 1,8‐diiodooctane (DIO), ethanolamine (NH2CH2CH2OH), and 2‐methoxyethanol (CH3OCH2CH2OH) were purchased from Sigma‐Aldrich. Other reagents and solvents were purchased from commercial sources and were used without further purification unless stated otherwise.
5
Synthesis and Characterization of P3HT-co-P3DDT
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We synthesized a P3HT-co-P3DDT using a Kumada catalyst transfer copolymerisation reaction involving LiCl promoted Grignard monomer activation. 47, 48 Protocols of synthesis and characterisations could be found in ESI. † 1,8-Diiodooctane (DIO) was purchased from Sigma-Aldrich. It was added as it is (as liquid) into the polymer solution (4% v/v) before spin-coating. Polymer nucleating agent 1,3:2,4-di(3,4-dimethylbenzylidene)sorbitol (DMDBS) was purchased from Chemos Gmbh and further used as it is (as solid powder) (1% w/w) into the solid polymer. The mixture was further dissolved in chlorobenzene, kept at 50 1C overnight while stirring, then filtered by 0.1 mm pore filter before spin-coating.
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