Tg dsc

Manufactured by Netzsch

Sourced in Germany

The TG/DSC is a thermal analysis instrument that simultaneously measures a sample's weight changes (Thermogravimetry - TG) and heat flow (Differential Scanning Calorimetry - DSC) as a function of temperature or time under a controlled atmosphere. This instrument provides quantitative information about physical and chemical changes that a material undergoes during heating or cooling.

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Lab products found in correlation

Sta 409 pc luxx, by Netzsch (2 mentions) Quanta 250 feg, by Thermo Fisher Scientific (1 mentions) Vertex 70 ftir spectrometer, by Bruker (1 mentions) Escalab 250xi, by Thermo Fisher Scientific (1 mentions) Fe sem, by Hitachi (1 mentions) Vertex 70 spectrometer, by Bruker (1 mentions)

Spelling variants of this product

TG-DSC simultaneous (2 citations) TG-DSC STA-449 F3 (2 citations) TG-DSC-STA 449 F3 Jupiter (2 citations) TG-DSC STA 499 F3 instrument (2 citations)

4 protocols using tg dsc

Oxidation Study of Yb-Lu-ZnSb

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Oxidation studies
of Yb_14–xLu_xZnSb₁₁ (x = 0.3) were performed
on pieces of dense pellets using
thermogravimetry and differential scanning calorimetry (TG/DSC, Netzsch
STA 449 Jupiter) under a 50 mL/min flow of dry air (20% oxygen in
N₂, Praxair) in Al₂O₃ crucibles from
room temperature to 1000 °C. To investigate the oxidation reaction
on a larger scale, a pellet of x = 0.3 was prepared
and after confirmation of purity by PXRD, the pellet was polished
and put in a box furnace in an Al₂O₃ holder.
It was heated at 200 °C/h to 1000 °C and held at that temperature
for 12 h in an ambient atmosphere. Half of this oxidized pellet was
set in epoxy for SEM imaging of the cross-section. The other half
was taken apart, the individual components were ground, and the PXRD
was collected and analyzed.

Justl A.P., Winston L.D., Bux S.K, & Kauzlarich S.M. (2023). Impact of Lu-Substitution in Yb14–xLuxZnSb11: Thermoelectric Properties and Oxidation Studies. ACS Applied Energy Materials, 6(20), 10628-10638.

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Maize Stalk Characterization Protocols

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Characterization of maize-stalk-loaded samples was done using a VERTEX 70 FTIR spectrometer (Bruker, Ettlingen, Germany) equipped with a diamond ATR accessory working at 4-cm⁻¹ resolution with 128 scans, a scanning electron microscope Quanta FEG 250 (Fei, Eindhoven, The Netherlands) and a STA 409 PC Luxx simultaneous thermogravimeter-differential scanning calorimeter TG/DSC (Netzsch, Selb, Germany) for thermal analysis. FTIR spectra were acquired in quadruplicate, using atmosphere background, the best-quality spectrum, automatically ranked by OPUS software for consideration to be used in the analysis.

Marin N.M., Dinu L., Stanculescu I., Cristea N.I, & Ionescu A.I. (2021). Maize Stalk Material for On-Site Treatment of Highly Polluted Leachate and Mine Wastewater. Materials, 14(4), 956.

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Comprehensive Characterization of Laminated AP Composite

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Field-emission scanning electron microscope (FESEM, Hitachi, Japan) was used to characterize the morphology, element mapping (EDS) and contents of the laminated AP composite. X-ray diffractometer (XRD, Bruker, Germany) was used to collect the XRD pattern of as-obtained samples. X-ray photoelectron spectra (XPS) were collected by an ESCALAB 250Xi photoelectron spectrometer (Thermo Fisher Scientific, USA). An BCA500 automatic oxygen bomb calorimeter was used to test the combustion heat value (IDEA SCIENCE, USA). The thermal decomposition properties of the samples were characterized by differential scanning calorimetry (TG-DSC, Netzsch, Germany) with the different heating rates (5, 10, 15, and 20 °C/min) in a Ar atmosphere over the temperature ranged from 25–600 °C.

Wang S., Guo X., Zhao W., Fang H., Wu C, & Wang D. (2021). Enhanced decomposition of laminated ammonium perchlorate composite. Scientific Reports, 11, 22622.

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Spectroscopic Characterization of AB 113 Dye

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The synthetic solutions of AB 113 used for adsorption, desorption and for biodegradation experiments were analyzed using a UV-Vis spectrometer from Hach Lange, Germany) in 1 cm quartz cells using the 200–800 nm. The spectra were recorded at 100 nm/min scanning speed for the ultrapure water in the adsorption experiment, acidic solutions for desorption experiment and dye-tampon buffer for biodegradation experiment. The pH buffer was measured with HI 255 Combined Meter (pH/mV & EC/TDS/NaCl) from Hanna Instruments, Nijverheidslaan, Belgium. The mass of IRA 402 and AB 113 powder was weighted with a XT220A analytical balance from Precisa Gravimetrics, Dietikon, Switzerland, with a precision of ±0.0004 g. For thermal analysis a STA 409 PC Luxx simultaneous thermogravimeter-differential scanning calorimeter TG/DSC from Netzsch, Selb, Germany was employed to verify AB 113 dye stability. FTIR spectra were acquired with a Vertex 70 spectrometer from Bruker, Ettlingen, Germany in transmittance mode in the 4000–400 cm⁻¹ range with 4 cm⁻¹ resolution and 32 scans.

Marin N.M, & Stanculescu I. (2021). Application of Amberlite IRA 402 Resin Adsorption and Laccase Treatment for Acid Blue 113 Removal from Aqueous Media. Polymers, 13(22), 3991.

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