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Xpert xrd

Manufactured by Philips

The Xpert XRD is a compact and versatile X-ray diffractometer designed for powder and thin-film analysis. It features a high-intensity X-ray source and a sensitive detector to provide accurate and reliable data on the crystallographic structure of materials. The Xpert XRD is a reliable tool for a wide range of research and industrial applications.

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2 protocols using xpert xrd

1

Comprehensive Materials Characterization

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The phase structure of the materials was studied by Philips Xpert XRD, applying CuKα radiation. The morphological features and chemical composition of the samples were characterized by LEO 1430 VP SEM/EDX instrument. The FT‐IR spectra were provided by a PerkinElmer Spectrum RX I instrument. The ultrasonic treatment was applied with a Bandelin ultrasound generator HD 3100.
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2

Cryo-Fractured Solid Characterization

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The X-Ray diffraction patterns, with 2Ɵ ranging from 6 to 40°, were collected in a XPert XRD (Philips, Eindohoven, The Netherlands) equipped with a high intensity ceramic sealed tube as the X-Ray source (3kW) and Cu K-α (with an energy of 8.04 keV and a wavelength of 1.54 Å ). Samples were placed inside a polyethylene terephthalate foil, needed for holding sample in place. Experiments were performed in transmission mode.
For the FTIR, Raman and X-Ray spectroscopic techniques, samples were immersed in liquid nitrogen and cryo-fractured prior to lyophilization. For FTIR and Raman special care was taken to analyze the core rather than surface of the samples to avoid artifacts related to sample manipulation or surface-induced changes.
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