Preparation of Fe(II) EDTA Solution: A 30 mM Fe(II) EDTA solution was prepared with equal molar Na2EDTA and FeSO4·7H2O.
Preparation of Fe(II) EDTA-NO Solution: A 30 mM Fe(II) EDTA solution was equally transferred into two absorption bottles, and N2 was used as protective gas to pass into NO gas to saturate the solution. The concentration of Fe(II) EDTA-NO was determined before use.
Na2EDTA·2H2O (99%), FeCl3·6H2O (99%), D-glucose (99.5%) and other chemicals were applied in analytical reagent grade without further purification, which were purchased from Sinopharm Chemical Reagent Co. (Shanghai, China). The compositions of simulated flue gas were supplied by Zhejiang Jingong Gas Co. (Hangzhou, China): N2 (99.999%), CO2 (99.999%), O2 (99.999%), and NO (5 vol% in N2).